| 高效液相色谱/质谱法检测人尿中的糖皮质激素及其它兴奋剂 |
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| 引用本文： | 秦旸,张建丽,王小兵,刘欣,王占良.高效液相色谱/质谱法检测人尿中的糖皮质激素及其它兴奋剂[J].中国运动医学杂志,2007,26(5):620-623. |
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| 作者姓名： | 秦旸 张建丽 王小兵 刘欣 王占良 |
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| 作者单位： | 国家体育总局运动医学研究所兴奋剂检测中心,北京,100029 |
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| 摘 要： | 采用液相色谱/质谱(LC/MS)方法检测糖皮质激素、甾体和β2激动剂。本文采用Zorbax 30 mm×2.1mm,1.8μm短柱,对12种糖皮质激素、3种甾体和2种β2激动剂的液相色谱/质谱的测定方法进行了研究,建立了6分钟内快速检测人尿中多种糖皮质激素、甾体和β2激动剂的测定方法。检测限低于5ng/ml。该方法适用于兴奋剂的筛选及确证。
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| 关 键 词： | 糖皮质激素 甾体 β2激动剂 高效液相色谱/质谱 人尿 |
| 修稿时间： | 2007年4月16日 |
Analysis of Glucocortisteroids and Some Other Dope Agents in Human Urine by Liquid Chromatography-Mass Spectrometry |
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| Qin Yang,Zhang Jianli,Wang Xiaobing,Liu Xin,Wang Zhanliang.Analysis of Glucocortisteroids and Some Other Dope Agents in Human Urine by Liquid Chromatography-Mass Spectrometry[J].Chinese Journal of Sports Medicine,2007,26(5):620-623. |
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| Authors: | Qin Yang Zhang Jianli Wang Xiaobing Liu Xin Wang Zhanliang |
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| Abstract: | Glucocortisteroids,anabolic steroids,and β2-agonists are all banned by WADA.The paper describes a procedure for simultaneous analysis of twelve glucocortisteroids,three anabolic steroids,and two β2-agonists in human urine with 6min by HPLC/MS with Zorbax rapid column.The detection limits of these compounds were below 5ng/ml.It is suitable for screening and confirmation in doping control. |
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| Keywords: | glucocortisteroids anabolic steroids β2-agonist HPLC/MS human urine |
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