| 毛瑞香化学成分研究 |
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| 引用本文： | 张薇,张卫东,李廷钊,张川,柳润辉,周耘,苏娟.毛瑞香化学成分研究[J].中国中药杂志,2005,30(7):513-515. |
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| 作者姓名： | 张薇 张卫东 李廷钊 张川 柳润辉 周耘 苏娟 |
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| 作者单位： | 第二军医大学,药学院,上海,200433 |
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| 基金项目： | 国家自然科学基金，上海市科技发展基金 |
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| 摘 要： | 目的:研究毛瑞香的化学成分。方法:应用色谱技术进行分离和纯化,通过光谱方法鉴定其化学结构。结果:得到16个化合物,鉴定其中的9个,分别为β谷甾醇(Ⅰ),对羟基苯甲酸乙酯(Ⅱ),反式2-丙烯酸3(3,4-二羟基苯基)二十二烷酯(Ⅲ),5,4′二羟基-7-甲氧基黄酮(即芫花素)(Ⅳ),2,4-二羟基嘧啶(Ⅴ),瑞香素(Ⅵ),双白瑞香素(Ⅶ),5,7,4′-三羟基黄酮-3醇(Ⅷ),β-胡萝卜苷(Ⅸ)。结论:化合物Ⅱ,Ⅲ,Ⅳ,Ⅴ,Ⅵ,Ⅷ,Ⅸ为首次从该植物中分得。
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| 关 键 词： | 瑞香属 毛瑞香 化学成分 |
| 文章编号： | 1001-5302(2005)07-0513-03 |
| 收稿时间： | 3/5/2004 12:00:00 AM |
Studies on the chemical constituents in roots of Daphne odora var. atrocaulis |
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| ZHANG Wei;ZHANG Wei-dong;LI Ting-zhao;ZHANG Chuan;LIU Run-hui;ZHOU Yun;SU Juan.Studies on the chemical constituents in roots of Daphne odora var. atrocaulis[J].China Journal of Chinese Materia Medica,2005,30(7):513-515. |
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| Authors: | ZHANG Wei;ZHANG Wei-dong;LI Ting-zhao;ZHANG Chuan;LIU Run-hui;ZHOU Yun;SU Juan |
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| Institution: | School of Pharmacy, Second Military Medical University, Shanghai 200433, China. |
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| Abstract: | OBJECTIVE: To study the chemical constituents from Daphne odora var. atrocaulis. METHOD: The chemical constituents were isolated and repeatedly purified by silica gel column chromatography and the structures were elucidated by the NMR spectra and physicochemical properties. RESULT: Sixteen compounds were obtained and nine of them were identified as beta-sitosterol, 4-hydroxy ethylbenzoate, (2E),-2-propenoic acid,3-(3,4-dihydroxyphenyl)-decosylester, genkwanin, 2,4-dihydroxypyrimidine, daphnetin, daphnoretin, 5,7,4'-trihydroxyflavone-3ol, daucosterol. CONCLUSION: Seven compounds were obtained from D. odora var. atrocaulis. for the first time. |
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| Keywords: | Daphne genus Daphne odora var atrocaulis chemical constituents |
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