| 10家医院饮片组方的茵陈蒿汤中11种成分的含量测定 |
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| 引用本文： | 窦志华,孟萍,姜晓燕,候金燕,顾薇,张琳,王征宇. 10家医院饮片组方的茵陈蒿汤中11种成分的含量测定[J]. 中国实验方剂学杂志, 2015, 21(23): 44-49 |
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| 作者姓名： | 窦志华 孟萍 姜晓燕 候金燕 顾薇 张琳 王征宇 |
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| 作者单位： | 南通大学附属南通第三医院, 江苏南通 226006,南通大学附属南通第三医院, 江苏南通 226006,南通市中医院, 江苏南通 226001,南京中医药大学, 南京 210023,南通大学附属南通第三医院, 江苏南通 226006,南通大学附属南通第三医院, 江苏南通 226006,南通大学附属南通第三医院, 江苏南通 226006 |
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| 基金项目： | 江苏省中医药局科技项目(HZ07071) |
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| 摘 要： | 目的:建立HPLC同时测定茵陈蒿汤中11种成分含量的方法。方法:采用高效液相色谱法,Symmetry C18色谱柱,流动相乙腈-0.1%磷酸梯度洗脱,流速1.0 m L·min~(-1),柱温30℃,检测波长254 nm。结果:来源于10家医院的茵陈蒿汤饮片组方中没食子酸、去乙酰车叶草酸甲酯、栀子苷、芦荟大黄素-8-O-葡萄糖苷、大黄酚-1-O-葡萄糖苷、大黄素-8-O-葡萄糖苷、芦荟大黄素、大黄酸、大黄素、大黄酚和大黄素甲醚的质量分数分别在0.142~1.016,0.518~1.256,9.021~17.214,0.088~0.793,0.097~0.990,0.187~1.587,0.057~0.578,0.147~1.062,0.114~0.730,0.380~1.898和0.375~1.958 mg·g-1。结论:不同来源中药饮片组成的茵陈蒿汤中活性成分的含量存在较大差异。
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| 关 键 词： | 茵陈蒿汤 没食子酸 环烯醚萜类 蒽醌 含量测定 高效液相色谱法 |
| 收稿时间： | 2015-04-05 |
Determination of 11 Constituents in Yinchenhao Tang Composed by Decoction Pieces from 10 Hospitals of Traditional Chinese Medicine |
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| DOU Zhi-hu,MENG Ping,JIANG Xiao-yan,HOU Jin-yan,GU Wei,ZHANG Lin and WANG Zheng-yu. Determination of 11 Constituents in Yinchenhao Tang Composed by Decoction Pieces from 10 Hospitals of Traditional Chinese Medicine[J]. China Journal of Experimental Traditional Medical Formulae, 2015, 21(23): 44-49 |
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| Authors: | DOU Zhi-hu MENG Ping JIANG Xiao-yan HOU Jin-yan GU Wei ZHANG Lin WANG Zheng-yu |
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| Affiliation: | Nantong Third Affiliated Hospital of Nantong University, Nantong 226006, China,Nantong Third Affiliated Hospital of Nantong University, Nantong 226006, China,Nantong Hospital of Traditional Chinese Medicine, Nantong 226001, China,Nanjing University of Chinese Medicine, Nanjing 210023, China,Nantong Third Affiliated Hospital of Nantong University, Nantong 226006, China,Nantong Third Affiliated Hospital of Nantong University, Nantong 226006, China and Nantong Third Affiliated Hospital of Nantong University, Nantong 226006, China |
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| Abstract: | |
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| Keywords: | Yinchenhao Tang gallic acid iridoids anthraquinones |
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