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HPLC法测定防已黄芪颗粒剂中防已诺林碱、粉防已碱的含量
引用本文:刘幸平,程康华,毕肖林,崔小兵,李伟,文红梅. HPLC法测定防已黄芪颗粒剂中防已诺林碱、粉防已碱的含量[J]. 南京中医药大学学报, 2001, 17(4): 230-231
作者姓名:刘幸平  程康华  毕肖林  崔小兵  李伟  文红梅
作者单位:1. 南京中医药大学药学院,
2. 南京林业大学化工学院,
3. 江苏省海洋药物研究开发中心,
基金项目:江苏省教委课题 (98KJD3 60 0 0 3 )
摘    要:目的:测定防已黄芪颗粒剂中防已诺林碱,粉防已碱的含量,方法:采用反相高效液相色谱法,结果:防已黄芪颗粒剂中已诺林碱,粉防已碱的含量,平均加样回收率分别已诺林碱:98.2%,RSD0.84%,粉防已碱:96.9%,RSD为1.45%,结论:本法简单,灵敏,结果可靠,可作为防已黄芪颗粒剂质量控制的定量方法。

关 键 词:防已黄芪颗粒剂 防已诺林碱 粉防已碱 反相高效液相色谱法 含量测定
文章编号:1000-5005(2001)04-0230-02
修稿时间:2001-03-04

HPLC Determination of Content of Fangchinoline and Tetrandrine in Radix Stephaniae Tetrandrae and Radix Astragali Seu Hedysari Granule
LIU Xing ping ,CHENG Kang hua ,BI Xiao lin ,CUI Xiao bing,LI Wei ,WEN Hong mei. HPLC Determination of Content of Fangchinoline and Tetrandrine in Radix Stephaniae Tetrandrae and Radix Astragali Seu Hedysari Granule[J]. Journal of Nanjing University of Traditional Chinese Medicine(Natural Science), 2001, 17(4): 230-231
Authors:LIU Xing ping   CHENG Kang hua   BI Xiao lin   CUI Xiao bing  LI Wei   WEN Hong mei
Affiliation:LIU Xing ping 1,CHENG Kang hua 2,BI Xiao lin 3,CUI Xiao bing3,LI Wei 3,WEN Hong mei 3
Abstract:OBJECTIVE To determine the content of fangchinoline and tetrandrine in Fangji Huangqi Granule. METHOD Reversed-phase HPLC method was used. RESULT The content of fangchinoline and tetrandrine and the average recovery rates were 98.2%, 0.84% and 96.9%, 1.45% respectively. CONCLUSION This method is simple and flexible with reliable results, and therefore can serve as the quantitative method for the quality control of Fangji Huangqi Granule.
Keywords:Fangji Huangqi Granule  fangchinoline  tetrandrine  Reversed phase HPLC
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