| 工作场所空气中28种挥发性有机物的气相色谱快速测定法 |
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| 引用本文： | 陈小丽,梁春霞,苏丹华,陈敏. 工作场所空气中28种挥发性有机物的气相色谱快速测定法[J]. 职业与健康, 2011, 27(7): 768-770 |
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| 作者姓名： | 陈小丽 梁春霞 苏丹华 陈敏 |
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| 作者单位： | 广州铁路疾病预防控制中心检验科,广东省广州市,510010 |
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| 基金项目： | 广铁(集团)公司科技项目 |
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| 摘 要： | 目的建立工作场所空气中28种挥发性有机物的快速测定方法。方法用活性炭采集工作场所空气中挥发性有机物,经二硫化碳解析后用毛细管气相色谱法测定。结果 28种挥发性有机物在一定浓度范围内线性关系良好,相关系数r>0.995,相对标准偏差为0.4%～6.5%,最低检出限远低于职业化学中毒现场剂量水平,目标组分平均解吸效率在77.3%～105.8%。结论方法准确度高,操作简便,灵敏快速,适用于工作场所空气中挥发性有机物的快速测定。
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| 关 键 词： | 挥发性有机物 工作场所空气 气相色谱法 |
Rapid determination of 28kinds of Volatile Organic Compounds in Workplace Air by Gas Chromatography |
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| CHEN Xiao-li,LIANG Chun-xia,SU Dan-hua,CHEN Min. Rapid determination of 28kinds of Volatile Organic Compounds in Workplace Air by Gas Chromatography[J]. Occupation and Health, 2011, 27(7): 768-770 |
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| Authors: | CHEN Xiao-li LIANG Chun-xia SU Dan-hua CHEN Min |
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| Affiliation: | CHEN Xiao-li,LIANG Chun-xia,SU Dan-hua,CHEN Min(Guangzhou Railway Center for Disease Control and Prevention,Guangdong,510010,China) |
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| Abstract: | [Objective]To establish a method for rapid determination of 28 kinds of volatile organic compounds in workplace air.[Methods]Volatile organic compounds in the air was adsorbed by activated carbon,desorbed by carbon bisulfide,then determined with capillary gas chromatography.[Results]The curve of 28 kinds of volatile organic compounds showed good linear relationship in a certain range.The correlation coefficient r0.995.The relative standard deviation（RSD） was 0.4%～6.5%.The detection limit was much more lower than poisoning dosage level in the workplace air,while the average desorption efficiency of target component was 77.3%～105.8%.[Conclusion]This method is accurate,simple,sensitive,rapid.It is suitable to detect volatile organic compounds in workplaceair. |
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| Keywords: | Volatile organic compounds Workplace air Gas chromatography |
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