| 正交试验法对大黄总蒽醌衍生物提取条件的优选 |
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| 引用本文： | 丁安伟,黄敏,孔令东,吴皓. 正交试验法对大黄总蒽醌衍生物提取条件的优选[J]. 中国中药杂志, 1988, 13(5): 37-39 |
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| 作者姓名： | 丁安伟 黄敏 孔令东 吴皓 |
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| 作者单位： | 南京中医学院中药系;1广西中医学院第一附属医院 |
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| 摘 要： | 对大黄中总蒽醌衍生物的提取方法做了某些改进,并使用正交试验法对提取条件进行优选.结果表明,以加入混合酸[冰HAc-25%HCl(10∶2)]20ml,水解2小时后氯仿提取较好。
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| 关 键 词： | 大黄 蒽醌 正交试验 |
Selection of the Extraction Conditions for Total Anthraquinone Derivatives in Rhubarb by Using Orthogonal Experiment Design |
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| Ding Anwei Huang Min Kong Lingdong and Wu Hao. Selection of the Extraction Conditions for Total Anthraquinone Derivatives in Rhubarb by Using Orthogonal Experiment Design[J]. China Journal of Chinese Materia Medica, 1988, 13(5): 37-39 |
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| Authors: | Ding Anwei Huang Min Kong Lingdong and Wu Hao |
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| Abstract: | The method of extraction for total anthraquinone derivatives in Rhubarb was improved in someaspects,and the extraction conditions were selected by using orthogonal experiment design.Theresult shows that a better way to extract the total anthraquinone derivatives is to add 20ml ofa mixed acid(glacial acetic acid:25 percent hydrochloric acid solution=10:2)to the powder ofRhubarb,let the latter hydrolyze for 2 hours and then proceed to extracting with chloroform. |
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| Keywords: | Rhubarb anthraquinone orthogonal experiment design |
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