| 蔓荆子中木脂素类成分的分离与结构鉴定 |
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| 引用本文： | 黄艳丽,张晗,郭颖,李安平,姚进龙,邓雁如,房士明.蔓荆子中木脂素类成分的分离与结构鉴定[J].天津中医药大学学报,2019,38(5):496-500. |
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| 作者姓名： | 黄艳丽 张晗 郭颖 李安平 姚进龙 邓雁如 房士明 |
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| 作者单位： | 天津中医药大学, 天津市中药化学与分析重点实验室, 天津 301617,天津中医药大学, 天津市中药化学与分析重点实验室, 天津 301617,天津南开医院, 天津 300100,瀚盟测试科技 (天津)有限公司, 天津 300457,天津中医药大学, 天津市中药化学与分析重点实验室, 天津 301617,天津中医药大学, 天津市中药化学与分析重点实验室, 天津 301617,天津中医药大学, 天津市中药化学与分析重点实验室, 天津 301617 |
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| 基金项目： | 国家高技术研究发展计划（"863"计划）资助项目（2013AA093001）。 |
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| 摘 要： | 目的]对蔓荆子中的木脂素类成分进行研究。方法]采用正相硅胶、Sephadex LH-20、MCI GEL(MCI)、反相ODS(ODS)等柱色谱及高效液相色谱手段进行分离纯化,并通过理化性质与波谱分析方法鉴定化合物的结构。结果]从蔓荆子95%乙醇提取物中分离得到7个木脂素类单体成分,分别为dihydrodehydrodiconiferyl alcohol(1),ficusal (2),(7R,8S)-dihydrodehydrodiconiferyl alcohol 9-O-β-D-glucopyranoside (3),dihydrodehydrodiconiferyl alcohol-β-D-(2′-O-p-hydroxybenzoyl)glucoside (4),(7R,8R)-7,8-dihydro-9′-hydroxyl-3′-methoxyl-8-hydroxymethyl-7-(4-hydroxy-3-methoxyphenyl)-1′-benzofuranpropanol 9′-O-β-D-glucopyranoside (5),松脂醇(pinoresinol)(6),1-syringaresinol(7)。结论]化合物5为首次从牡荆属中分离得到,化合物6和7为首次从该植物中分离得到的化合物。
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| 关 键 词： | 蔓荆子 木脂素 化学成分 结构鉴定 |
| 收稿时间： | 2019/5/25 0:00:00 |
Isolation and structural identification of lignans from fruits of Vitex trifolia L. var. simplicifolia Cham. |
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| HUANG Yanli,ZHANG Han,GUO Ying,LI Anping,YAO Jinlong,DENG Yanru and FANG Shiming.Isolation and structural identification of lignans from fruits of Vitex trifolia L. var. simplicifolia Cham.[J].Journal of Tianjin University of Traditonal Chinese Medicine,2019,38(5):496-500. |
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| Authors: | HUANG Yanli ZHANG Han GUO Ying LI Anping YAO Jinlong DENG Yanru and FANG Shiming |
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| Institution: | Tianjin University of Traditional Chinese Medicine, Key Laboratory of Traditional Chinese Medicinal Chemistry and Analytical Chemistry of Tianjin, Tianjin 300193, China,Tianjin University of Traditional Chinese Medicine, Key Laboratory of Traditional Chinese Medicinal Chemistry and Analytical Chemistry of Tianjin, Tianjin 300193, China,Tianjin Nankai Hospital, Tianjin 300100, China,Harmonia Testing(Tianjin) Co., Ltd, Tianjin 300457, China,Tianjin University of Traditional Chinese Medicine, Key Laboratory of Traditional Chinese Medicinal Chemistry and Analytical Chemistry of Tianjin, Tianjin 300193, China,Tianjin University of Traditional Chinese Medicine, Key Laboratory of Traditional Chinese Medicinal Chemistry and Analytical Chemistry of Tianjin, Tianjin 300193, China and Tianjin University of Traditional Chinese Medicine, Key Laboratory of Traditional Chinese Medicinal Chemistry and Analytical Chemistry of Tianjin, Tianjin 300193, China |
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| Abstract: | |
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| Keywords: | Vitex Fructus lignans chemical constituents structural identification |
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