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| HPLC法测定抗骨增生片中柚皮苷含量 | |
| 引用本文： | 张智军,崔华,马久太. HPLC法测定抗骨增生片中柚皮苷含量[J]. 世界中医药, 2012, 7(4): 360-361 |
| 作者姓名： | 张智军 崔华 马久太 |
| 作者单位： | 1. 彬县食品药品监督管理局,陕西省彬县西大街老政府院内,713500 2. 陕西摩美得制药有限公司 3. 陕西步长制药有限公司 |
| 摘 要： | 目的:建立抗骨增生片中柚皮苷含量测定方法。方法:采用HPLC法,C18柱色谱柱,流动相乙腈-水-冰醋酸(14:86:4),流速1.0mL·min-1,检测波长283nm,柱温40℃。结果:在0.0284～0.0994μg范围内柚皮苷线性关系良好,平均回收率为98.76%,RSD为0.68%。结论:该方法能够对抗骨增生片进行准确、快速的柚皮苷定量检测。 |
| 关 键 词： | HPLC 抗骨增生片 柚皮苷 |
| 收稿时间： | 2012-04-11 |
Determination of the content of naringin in Kanggu Zengsheng Tablet by HPLC |
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| Zhang Zhijun,Cui Hu,Ma Jiutai. Determination of the content of naringin in Kanggu Zengsheng Tablet by HPLC[J]. World Chinese Medicine, 2012, 7(4): 360-361 | |
| Authors: | Zhang Zhijun Cui Hu Ma Jiutai |
| Affiliation: | 1 Binxian Food And Drug Administration, Binxian, Post code： 713500;2 Shaanxi Momentum Pharmaceutical Co. , LTD; 3 Shaanxi Buchang Pharmaceutical Co. ,LTD ) |
| Abstract: | Objective：The method was established for determination of the content of naringin in Kanggu Zengsheng Tablet. Methods： C18 column was used with gradient elution of Acetonitrile - water - glacial acetic acid （ 14：86：4） as mobile phase by flow rate of 1.0 mL· min-1. The detection wavelength was 283nm and the column temperature was 40℃. Results： The cabibration curves of naringin was in good linearity over the range of 0. 0284 -0. 0994μg （r = 0. 9999 ）. The average rccoverage of naringin was 98.76% （n = 6, RSD 0. 68% ）. Conclusion： The method is accurate and quick for determinating the content of naringin in Kanggu Zengsheng Tablet. |
| Keywords: | HPLC Kanggu Zengsheng Tablet Naringin |
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