| 不同树脂富集雷公藤内酯醇的比较 |
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| 引用本文： | 王曙东,汤湝,李克. 不同树脂富集雷公藤内酯醇的比较[J]. 医学研究生学报, 2007, 20(6): 572-573,577 |
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| 作者姓名： | 王曙东 汤湝 李克 |
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| 作者单位： | 1. 南京军区南京总医院,制剂科,江苏,南京,210002
2. 南京军区南京总医院,解放军临床检验医学研究所,江苏,南京,210002 |
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| 基金项目： | 江苏省六大人才高峰基金 |
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| 摘 要： | 目的：选择适合富集雷公藤内酯醇的树脂。方法：药液分别用3种极性树脂富集，以95％乙醇洗脱，高效液相色谱（HPLC）法测定含量，同时测定醇洗液的含固量。结果：D101型树脂更适宜于富集雷公藤内酯醇。结论：D101型树脂可用于雷公藤内酯醇的富集。
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| 关 键 词： | 大孔吸附树脂 雷公藤内酯醇 高效液相色谱 含固量 |
| 文章编号： | 1008-8199（2007）06-0572-02 |
| 收稿时间： | 2006-05-09 |
| 修稿时间： | 2006-05-092007-02-06 |
Comparison of different macroporous adsorbing resins for triptolide enrichment |
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| WANG Shu-dong,TANG Hao,LI Ke. Comparison of different macroporous adsorbing resins for triptolide enrichment[J]. Bulletin of Medical Postgraduate, 2007, 20(6): 572-573,577 |
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| Authors: | WANG Shu-dong TANG Hao LI Ke |
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| Affiliation: | 1. Department of Preparation; 2. Institute of Laboratory Medicine Science of PLA, Nanjing General Hospital of Nanjing Military Command, PLA , Nanjing 210002, Jiangsu , China |
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| Abstract: | Objective:To select proper macroporous resins for enrichment triptolide.Methods:Experiments were performed to adsorb triptolide by three types macroporous resins.Then the triptolide and solide content on the columns were eluated with 95% alcohol and determined by HPLC.Results:Results showed that the macroporous of type D101 is the best choice for enrichment of triptolide.Conclusion:the macroporous of type D101 can be used for triptolide enrichment. |
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| Keywords: | Macroporous adsorbing resins Triptolide High-performance liquid chro-matography Solide content |
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