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芪花生肌胶囊的质量标准研究
引用本文:王志锋,高鸿英,于武高. 芪花生肌胶囊的质量标准研究[J]. 甘肃中医学院学报, 2011, 28(5): 42-45
作者姓名:王志锋  高鸿英  于武高
作者单位:1. 甘肃新兰药药业有限公司,甘肃兰州,730046
2. 兰州大得利生物化学制药有限公司,甘肃兰州,730046
摘    要:目的 制订芪花生肌胶囊的质量控制方法.方法 采用薄层色谱法(TLC)对芪花生肌胶囊方中当归、金银花进行鉴别,采用高效液相色谱法( HPLC)测定芪花生肌胶囊中黄芪甲苷的含量.结果 TLC鉴别方法专属性强;黄芪甲苷线性范围为0.996 ~9.960 μg(r =0.999 8),平均回收率为97.90%,RSD为1.77...

关 键 词:芪花生肌胶囊  质量标准  TLC  HPLC  黄芪甲苷

Study of quality standard of Qihua Shengji Capsule
Wang Zhifeng,Gao Hongying,Yu Wugao. Study of quality standard of Qihua Shengji Capsule[J]. Journal of Gansu College of Traditional Chinese Medicine, 2011, 28(5): 42-45
Authors:Wang Zhifeng  Gao Hongying  Yu Wugao
Affiliation:1(1.Gansu Pharmaceutical Limited Company of Xinlan Medicine,Lanzhou 730046,China; 2.Lanzhou Dadeli Limited Company of Biochemical Pharmaceutical,Lanzhou 730046,China)
Abstract:Objective To consummate a method for quality control of Qihua shengji Capsule.Methods TLC was used for the identification of Angelica sinensis and Lonicera japonica,and HPLC was used for the determination of astragaloside in Qihua shengji Capsule.Results The TLC identification method was highly specific and the spots were clear.The linear range of astragaloside was from 0.996 to 9.960 μg(r=0.999 8).The average recovery of astragaloside was 97.9%,RSD was 1.77%(n=6).Conclusion The method is easy to operate with accurate results,high sensitivity and good reproducibility.The quality standard can effectively control the quality of Qihua shengji Capsule.
Keywords:Qihua shengji Capsule  quality standard  TLC  HPLC  astragaloside
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