| HPLC法测定芩连片中连翘苷的含量 |
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| 引用本文： | 迟芳振,丁始阳,王金洲.HPLC法测定芩连片中连翘苷的含量[J].中国药师,2010,13(5):688-689. |
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| 作者姓名： | 迟芳振 丁始阳 王金洲 |
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| 作者单位： | 烟台药品检验所,山东烟台,264000 |
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| 摘 要： | 目的：采用高效液相色谱法测定芩连片中连翘苷的含量。方法：色谱柱为Hypersil C18（150mm×4．6mm，5μm），以乙腈-水（25：75）为流动相，流速1．0ml·min^-1，检测波长277nm。结果：连翘苷进样量在0．20～1．61μg范围内与峰面积具有良好的线性关系，r为0．9999，回收率98．0％（RSD=0．98％，n=6）。结论：方法操作简便，精密度好，结果准确可靠，适用于芩连片中连翘苷含量的测定。
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| 关 键 词： | 高效液相色谱法 连翘苷 芩连片 |
Determination of Forsythin in Qinlian Tablets by HPLC |
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| Chi Fangzhen,Ding Shiyang,Wang Jinzhou.Determination of Forsythin in Qinlian Tablets by HPLC[J].China Pharmacist,2010,13(5):688-689. |
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| Authors: | Chi Fangzhen Ding Shiyang Wang Jinzhou |
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| Institution: | ( Yantai Institute for Drug Control, Shangdong Yantai 264000, China ) |
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| Abstract: | Objective ： To determine Content of Forsythin in Qin lian Tablets by HPLC. Method： The Hypersill BDS C18 （ 150 mm ×4.6 mm,5 μm） was used, the Acctonitrile-Water （25： 75） as mobile phase ,the flow rate was 1.0 ml · min^-1 , the detection wavelength was 277 nm. Result： The calibration curve was linear in the range of 0.20-1.61 μg for Forsythin （r = 0.999 9 ） , the average reeovevery was 98.0% （RSD 0. 98% ,n = 6）. Conclusion： The method is rapid, accurate and reliable, it suitable for determination of forsyhin in Qin lian Tablets. |
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| Keywords: | HPLC Forsythin Qinlian Tablets |
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