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薯莨块茎脂肪酸和挥发油成分的GC-MS分析
引用本文:李晓菲,宋文东,纪丽丽,刘娟花,仝绍伟,安静波.薯莨块茎脂肪酸和挥发油成分的GC-MS分析[J].中国实验方剂学杂志,2012,18(4):129-131.
作者姓名:李晓菲  宋文东  纪丽丽  刘娟花  仝绍伟  安静波
作者单位:1. 广东海洋大学,广东湛江,524088
2. 东华大学环境科学与工程学院,上海,200051
摘    要:目的:分析测定薯莨Dioscorea Cirrhosa Lour.块茎中的脂肪酸和挥发油的含量及种类.方法:采用气相色谱-质谱联用仪进行测定.结果:从脂肪酸组份中分离出50个峰,鉴定出12种脂肪酸,其中主要成分有9,12-十八碳二烯酸(亚油酸,21.59%)、十六酸(棕榈酸,16.22%)等;挥发油组分中分离出32个峰,鉴定出32种化合物,其中间甲基苯酚、苯酚、2-甲基苯酚含量较高,分别占挥发油总量的26.92%,18.95%,12.12%.结论:对薯莨块茎中脂肪酸、挥发性组分进行了分析测定,为进一步综合开发利用薯莨提供了一定的理论依据.

关 键 词:薯莨  脂肪酸  挥发油  GC-MS

Study on Volatile Oil and Fatty Acids from Dioscorea cirrhosa by GC-MS
LI Xiao-fei,SONG Wen-dong,JI Li-li,LIU Juan-hu,TONG Shao-wei and AN Jing-bo.Study on Volatile Oil and Fatty Acids from Dioscorea cirrhosa by GC-MS[J].China Journal of Experimental Traditional Medical Formulae,2012,18(4):129-131.
Authors:LI Xiao-fei  SONG Wen-dong  JI Li-li  LIU Juan-hu  TONG Shao-wei and AN Jing-bo
Institution:Guangdong Ocean University, Zhanjiang 524088, China;Guangdong Ocean University, Zhanjiang 524088, China;School of Environment Science and Engineering, Donghua University, Shanghai 200051, China;Guangdong Ocean University, Zhanjiang 524088, China;Guangdong Ocean University, Zhanjiang 524088, China;Guangdong Ocean University, Zhanjiang 524088, China
Abstract:Objective: The volatile oil and fatty acid of the Dioscorea cirrhosa. were analyzed. Method: In this study, the capillary GC-MS was used. Result: Fifty peaks were separated,12 compounds were identified from the fatty acids, the tuber of D. cirrhosa contained abundant octadecadienoic acid and hexadecanoic acid, they were 21.59% and 16.22%of total fatty acids respectively.And 32 peaks were separated and 32 compounds were identified from the volatile oil, m-cresol (26.92%), phenyl hydroxide (18.95%), o-cresylic acid(12.12%) were the dominant constituents. Conclusion: The results provide the scientific basis for comprehensive development and utilization of D. Cirrhosa .
Keywords:Dioscorea cirrhosa  fatty acid  volatile oil  GC-MS
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