| HPLC测定荆菊感冒片中牛蒡苷的含量 |
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| 引用本文： | 廖晓鸣,郑丹,宋志娟,马仁强.HPLC测定荆菊感冒片中牛蒡苷的含量[J].中国实验方剂学杂志,2012,18(4):113-115. |
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| 作者姓名： | 廖晓鸣 郑丹 宋志娟 马仁强 |
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| 作者单位： | 1. 深圳市康哲药业有限公司,广东深圳,518057
2. 广州博济医药生物技术有限公司,广州 ,510620 |
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| 摘 要： | 目的:建立荆菊感冒片中牛蒡苷的含量测定方法.方法:采用高效液相色谱法,以VARIAN Microsorb 100-5 C18柱为分析柱,甲醇-水(40∶60)为流动相,流速1.0 mL·min-1,检测波长为280 nm.结果:牛蒡苷在0.0428 ～0.856 g·L-1线性关系良好,r=0.999 9；平均加样回收率为100.2％,RSD 1.45％ (n =6).结论:该方法简便、快速、准确,可用于测定荆菊感冒片中牛蒡苷的含量.
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| 关 键 词： | 荆菊感冒片 牛蒡苷 高效液相色谱法 |
Determination of Arctiin in Jingju Ganmao Tablets by HPLC |
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| LIAO Xiao-ming,ZHENG Dan,SONG Zhi-juan and MA Ren-qiang.Determination of Arctiin in Jingju Ganmao Tablets by HPLC[J].China Journal of Experimental Traditional Medical Formulae,2012,18(4):113-115. |
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| Authors: | LIAO Xiao-ming ZHENG Dan SONG Zhi-juan and MA Ren-qiang |
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| Institution: | Shenzhen Kangzhe Pharmaceutical Co.,Ltd, Shenzhen 518057, China;Guangzhou Boji Medicinal and Biological Technology Co. Ltd, Guangzhou 510620, China;Guangzhou Boji Medicinal and Biological Technology Co. Ltd, Guangzhou 510620, China;Guangzhou Boji Medicinal and Biological Technology Co. Ltd, Guangzhou 510620, China |
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| Abstract: | Objective:To establish a HPLC method to determine arctiin in Jingju Ganmao tablets.Method:The determination was conducted by HPLC using a VARIAN Microsorb 100-5 C18 column.The mobile phase consisted of CH3OH∶ H2O(40∶ 60) with flow rate of 1.0 mL.min-1 and the detection wavelength was 280 nm.Result:This method had good resolution and good linear relationship between 0.042 8-0.856 g.L-1.The averagere covery of arctiin was 100.2% and RSD was 1.45%(n=6).Conclusion:This method is simple,quick and accurate.It can be used for quantity control of Jingju Ganmao tablets. |
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| Keywords: | Jingju Ganmao tablet arctiin HPLC |
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