| 肝乐舒颗粒的质量标准研究 |
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| 引用本文： | 曹军,杨静,陈雷,杨志福,王磊,李华,崔佳,文爱东.肝乐舒颗粒的质量标准研究[J].中国药师,2012,15(8):1111-1113. |
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| 作者姓名： | 曹军 杨静 陈雷 杨志福 王磊 李华 崔佳 文爱东 |
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| 作者单位： | 第四军医大学西京医院药剂科,西安,710032 |
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| 摘 要： | 目的:建立肝乐舒颗粒的质量标准.方法:采用TLC法对方中的灵芝、五味子进行定性鉴别;采用HPLC法对处方中的丹参酮ⅡA进行含量测定.结果:TLC斑点清晰、分离度好、专属性强,阴性对照无干扰;丹参酮ⅡA的进样量在0.2～4.0 μg范围内与峰面积积分值呈良好线性关系,平均回收率98.34%,RSD=1.86%(n=5).结论:所建标准能有效控制肝乐舒颗粒的质量.
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| 关 键 词： | 肝乐舒颗粒 质量标准 薄层色谱法 高效液相色谱法 |
| 收稿时间： | 2012/3/20 0:00:00 |
| 修稿时间： | 5/2/2012 12:00:00 AM |
Study on Quality Standard of Ganleshu Granules |
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| Cao Jun,Yang Jing,Chen Lei,Yang Zhifu,Wang Lei,Li Hu,Cui Jia and Wen Aidong.Study on Quality Standard of Ganleshu Granules[J].China Pharmacist,2012,15(8):1111-1113. |
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| Authors: | Cao Jun Yang Jing Chen Lei Yang Zhifu Wang Lei Li Hu Cui Jia and Wen Aidong |
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| Institution: | ( Department of Pharmacy, Xijing Hospital, the Fourth Military Medical University, Xian 710032, China) |
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| Abstract: | Objective ： To establish the quality standard of Ganlesh, n granules. Method： TLC was employed to identify Ganoderma lucidum and Schisandra chinensis. Tanshinone IIs in Ganleshu granules was determined by HPLC. Result： TLC spots were clear, well - separated and specific without interference of the negative control. The linear range of tanshinone ⅡA was 0.2 - 4.0 p,g with the average recovery of 98.34% （ RSD = 1.86% , n = 5 ）. Conclusion： The established standard is suitable for the quality control of Ganleshu ganules. |
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| Keywords: | Ganleshu granules Quality standard TLC HPLC |
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