| 高效液相色谱法测定板蓝根颗粒中表告依春含量 |
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| 引用本文： | 崔田,张祖亮. 高效液相色谱法测定板蓝根颗粒中表告依春含量[J]. 中国药业, 2012, 21(8): 50-51 |
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| 作者姓名： | 崔田 张祖亮 |
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| 作者单位： | 1. 安徽省蚌埠市食品药品检验所,安徽蚌埠,233000
2. 安徽省六安市食品药品检验所,安徽六安,237006 |
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| 摘 要： | 目的 建立测定板蓝根颗粒中表告依春含量的高效液相色谱法.方法 色谱柱为Kromasil C18柱(250mm×4.6mm,5μm),流动相为甲醇-水(15:85),流速为1.0 mL/min,检测波长为245 nm,柱温为30℃.结果 表告依春进样量在0.010~0.516 μg(r=0.999 9)范围内与峰面积线性关系良好,平均加样回收率为99.16%,RSD为0.86%(n=6).结论 该方法简便快速、结果准确,可以有效控制药品质量.
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| 关 键 词： | 高效液相色谱法 板蓝根颗粒 表告依春 |
Determination of Epigoitrin in Banlangen Granules by HPLC |
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| Cui Tian , Zhang Zulian. Determination of Epigoitrin in Banlangen Granules by HPLC[J]. China Pharmaceuticals, 2012, 21(8): 50-51 |
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| Authors: | Cui Tian Zhang Zulian |
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| Affiliation: | 1. Anhui Bengbu Institute for Food and Drug Control, Bengbu, Anhui, China 233000; 2. Anhui Liaan Institute for Food and Drag Control, Liuan, Anhui, China 237006) |
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| Abstract: | Objective Aim To establish an HPLC method for the determinatione of epigoitrin in Banlangen Granules. Methods The HPLC method was used with the Kromasil C18（250 mm ×4.6 mm,5 μm）and the mobile phase of methanol - water（15：85）.The flow rate was set at 1.0 mL/min. The detection wavelength was at 245 nm. Column temperature was 30 ℃. Results The linear of epigoitrin was 0. 010-0. 516 μg（r =0. 999 9）, and the average recovery was 99. 16% with the RSD was 0. 86% （n =6）. Conclusion The method is convenient, rapid, and accurate. It can be used for the quality control of the drug. |
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| Keywords: | HPLC Banlangen Granules epigoitrin |
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