| 固相微萃取气质联用测定中药辛夷挥发性成分 |
| |
| 引用本文： | 王琦,齐美玲,傅若农. 固相微萃取气质联用测定中药辛夷挥发性成分[J]. 世界科学技术, 2009, 11(1): 168-172 |
| |
| 作者姓名： | 王琦 齐美玲 傅若农 |
| |
| 作者单位： | 北京理工大学理学院化学系,北京,100081 |
| |
| 摘 要： | 本研究采用固相微萃取气质联用（SPME—GC—MS）测定了中药辛夷挥发性成分。研究结果表明，采用混合涂层PDMS／DVB／CAR，在80℃下对0．5g药材粉末样品顶空萃取30min后进行GC—MS分析可获得令人满意的测定结果。同水蒸气蒸馏法相比，本法具有简便、快速、样品量小等特点，适于中药挥发性成分的快速测定。
|
| 关 键 词： | 固相微萃取 GC—MS法 辛夷 |
Analysis of volatile compounds in Magnolia biondii Pamp by SPME-GC-MS |
| |
| Wang Qi,Qi Meiling,Fu Ruonong. Analysis of volatile compounds in Magnolia biondii Pamp by SPME-GC-MS[J]. World Science and Technology(Modernization of Traditional Chinese Medicine), 2009, 11(1): 168-172 |
| |
| Authors: | Wang Qi Qi Meiling Fu Ruonong |
| |
| Affiliation: | (Department of Chemistry, School of Science, Beijing Institute of Technology, Beijing 100081) |
| |
| Abstract: | The present work describes a solid-phase microextraction-gas chromatography- mass spectrometry （SPME-GC- MS） for the analysis of volatile compounds in Magnolia biondii Pamp. The optimum SPME was achieved by using PDMS/DVB/CAR fiber over 0.5g of the powdered sample at 80℃ for 30min. In comparison with traditional steam distillation, the proposed method is simple, rapid and less sample-demanding and can be used for the fast analysis of volatile compounds in traditional Chinese medicines. |
| |
| Keywords: | Solid-phase microextraction GC-MS Magnolia biondii Pamp |
| 本文献已被 维普 万方数据 等数据库收录！ |
|
