| GC/MS检测桑白皮的农药残留 |
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| 引用本文： | 黄丽娜,何昱. GC/MS检测桑白皮的农药残留[J]. 中华中医药学刊, 2014, 0(3): 652-654 |
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| 作者姓名： | 黄丽娜 何昱 |
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| 作者单位： | [1]浙江中医药大学附属第二医院,浙江杭州310005 [2]浙江中医药大学,浙江杭州310053 |
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| 摘 要： | 目的:检测桑白皮样品中的农药残留情况,确保药材质量。方法:用气质联用(GC-MS)法快速测定桑白皮样品的多种农药。采用不分流进样模式;进样口采用程序升温:120℃(4.5 min)按80℃/min至250℃(34 min);柱温箱程序升温:82℃(5 min)按8℃/min至280℃;柱流速控制:恒压120 Mpa;载气总流速:30 mL/min;柱流速:1.75 mL/min。MS离子源温度:200℃;接口温度:250℃;质谱检测模式:SIM。结果:对检测的样品进行分析发现,其中具有农药残留,并且虫螨畏含量很高。结论:样品中含有虫螨畏残留,可确定在生产过程中虫螨畏污染比较严重。
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| 关 键 词： | 桑白皮 气质联用 农药残留 |
Detection of Pesticide Residues in Morus Alba Using GC- MS |
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| HUANG Lina,HE Yu. Detection of Pesticide Residues in Morus Alba Using GC- MS[J]. Chinese Archives of Traditional Chinese Medicine, 2014, 0(3): 652-654 |
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| Authors: | HUANG Lina HE Yu |
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| Affiliation: | 1 The Secend Hospital Affiliated to Zhejiang Chinese Medical University, Hangzhou 310005, Zhejiang, China; 2. Zhejiang University of Traditional Chinese Medicine, Hangzhou 310005, Zhejiang, China) |
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| Abstract: | Objective ：To to determine the situation of pesticide residues in Morus Alba to ensure the quality of it. Methods ： GC - MS was used to determine multiresidue pesticide in Morus Alba samples. Splitless injector was operated in pulsed - splitless mode. Inlet temperature program ： 120 ℃ （ initial isotherm ：4.5 min） up to 250 ℃ at a rate of 80℃/ min;oventemperature program： 82 % （initial isotherm：5 min） up to 280 ℃ at a rate of 8 ℃/min;column flow rate： constant pressure 120 Mpa; carrier gas flow rate ：300 mL/min ; column flow rate ： 1.75 mL/min ; Ion source temperature ： 200℃; interface temperature ： 250 ℃ ; MS detection mode ： SIM. Results ： Detection of the sample analysis can find pesti- cide residues and high levels of methacrifos. Conclusion：The sample has methacrifos residues and it can be determined that methacrifos was used during the plant growth process . |
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| Keywords: | Morus Alba gas chromatography mass spectrometry pesticide residues |
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