| 正交试验法优选吴茱萸酸水提取工艺 |
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| 引用本文： | 逯振宇,秦序锋,朱方剑,姚瑶,林丽萍.正交试验法优选吴茱萸酸水提取工艺[J].河南中医学院学报,2011,26(2). |
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| 作者姓名： | 逯振宇 秦序锋 朱方剑 姚瑶 林丽萍 |
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| 作者单位： | 浙江佐力药业有限公司研发部; |
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| 摘 要： | 目的:用正交实验提取吴茱萸中有效成分吴莱萸碱,优选吴茱萸的提取路线。方法:采用高效液相色谱(HPLC)法测定吴茱萸酸水提物中吴茱萸碱的含量,求出最佳条件。结果:实验表明,酸水浓度、浸泡时间对吴茱萸碱的提取影响较大,煎煮时间则次之。结论:经筛选,吴莱萸中生物碱水提取的工艺路线为:吴茱萸浸泡1.5 h、煎煮30 min、醋酸浓度为1%,在此条件下吴茱萸中生物碱提取完全。
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| 关 键 词： | 吴茱萸碱 中药提取工艺 正交试验法 |
Extraction Processing of Evodia Acidic Water Optimized with Orthogonal Test |
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| Lu Zhen-yu,Qin Xu-feng,Zhu Fang-jian,Yao Yao,Lin Li-ping.Extraction Processing of Evodia Acidic Water Optimized with Orthogonal Test[J].Journal of Henan University of Chinese Medicine,2011,26(2). |
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| Authors: | Lu Zhen-yu Qin Xu-feng Zhu Fang-jian Yao Yao Lin Li-ping |
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| Institution: | Lu Zhen-yu Qin Xu-feng Zhu Fang-jian Yao Yao Lin Li-ping Zhejiang Jolly Pharmaceutical Co.,Ltd.,Huzhou,Zhejiang,China 313200 |
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| Abstract: | Objective:To Extract rutaecarpine which is the effective component in Evodia rutaecarpa by orthogonal experiment and then optimize the extracting course.Methods:To determine the content of rutaecarpine which was extracted from the aqueous extract of xanthoxylic acid and work out the optimum condition through the way of HPLC.Results:The experiment showed that decoction time and menstruum dosage had more significant influence on extracting rutaecarpine,and decoction hour took the second place.Conclusion:Throu... |
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| Keywords: | Evodia rutaecarpm extracting processing of chinese herbs orthogonal design |
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