| HPLC法测定肿痛消喷雾剂中人参皂苷Rg1、三七皂苷R1含量 |
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| 引用本文： | 曲静,刘丽,王艳春.HPLC法测定肿痛消喷雾剂中人参皂苷Rg1、三七皂苷R1含量[J].中国民族民间医药杂志,2011,20(1):48-49. |
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| 作者姓名： | 曲静 刘丽 王艳春 |
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| 作者单位： | 曲静,刘丽,Qujing,Liuli(辽宁中医药大学,辽宁,沈阳,110032);王艳春,Wang Yanchun(辽宁中医药大学附属医院,辽宁,沈阳,110032) |
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| 摘 要： | 目的：建立肿痛消喷雾剂中人参皂苷Rg1、三七皂苷R1的含量测定方法。方法：色谱柱：C18（200×4．6mm，5μm）；流动相：乙腈-水-磷酸（20：80：0．05）；流速：1．0mL／min；检测波长：203nm。结果：人参皂苷Rg1在1．844—9．220μg范围内线性关系良好；三七皂苷R1在0．892—4．46μg范围内线性关系良好。结论：本方法简便、准确，重复性好，可作为肿痛消喷雾剂的质量控制方法。
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| 关 键 词： | 肿痛消喷雾剂 人参皂苷Rg1 三七皂苷R1 高效液相色谱法 |
Determination of ginsenoside Rg1 and notoginsenoside R1 Contents in Zhongtongxiao Spray by HPLC |
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| Qujing,Liuli,Wang Yanchun.Determination of ginsenoside Rg1 and notoginsenoside R1 Contents in Zhongtongxiao Spray by HPLC[J].Chinese Journal of Ethnomedicine and Ethnopharmacy,2011,20(1):48-49. |
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| Authors: | Qujing Liuli Wang Yanchun |
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| Institution: | 1, 2 Liaoning University of Traditional Chinese Medicine; 3 Liaoning University of Traditional Chinese Medicine Hospital) |
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| Abstract: | Objective： To establish a HPLC method for determination ginsenoside Rgl and notoginsenoside R1 in Zhongtongxiao Spray. Method： The column was C18 （200 ×4.6mm,5μm） . The mobile phase was acetonitrile -water - phosphoric acid （20： 80 ： 0. 05 ） and the flow rate was 1.0 mL/min. The detection wavelength was at 203 nm. Results ： Ginsenoside Rgl has a good linear between 1. 844 -9. 22μg and Notoginsenoside R1 has a good linear between 0. 892 -4. 46μg. Conclusion： The method is smiple and accurate with good repeatability and can be used for the quality control of ginsenoside Rgl and Notoginsenoside RI in Zhongtongxiao Spray. |
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| Keywords: | Zhongtongxiao Spray ginsenoside Rg1 notoginsenoside R1 HPLC |
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