| 中药保健品苦瓜素胶囊中非法添加格列本脲的快速检测方法 |
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| 引用本文： | 葛海生,于玲,杜华霜,王晓飞.中药保健品苦瓜素胶囊中非法添加格列本脲的快速检测方法[J].中国民族民间医药杂志,2011,20(4):22-23,25. |
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| 作者姓名： | 葛海生 于玲 杜华霜 王晓飞 |
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| 作者单位： | 武警部队药品仪器检验所,北京,102613 |
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| 摘 要： | 目的：考察建立一种测定中药保健品苦瓜素胶囊中非法添加格列本脲的快速检测方法。方法：建立薄层色谱法初步筛选、高效液相色谱法对可能添加格列本脲的中药保健品苦瓜素胶囊进行分离分析，并用高效液相色谱法一二极管阵列进行定性鉴别，再采用高效液相色谱法测定其中格列本脲的含量。结果：苦瓜素胶囊中检出格列本脲，含量为3．38μg／g）。结论：本法可用于快速检测中药保健品中添加的格列本脲。
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| 关 键 词： | 中药保健品 苦瓜素胶囊 格列本脲 薄层色谱法 高效液相色谱法 |
Fast Determination of Glibenclamide Added Illegally in kuguasu Capsules of Traditional Chinese Medicine for health care |
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| Abstract: | Objective:To establish a method for fast identification of illegal adding of Glibenclamide in kuguasu Capsules of Traditional Chinese Medicine for health care.Method:TLCS was used in initial screening.HPLC methods was establish for the separation and determination of the organic extract in kuguasu Capsules of Traditional Chinese Medicine for health care,Glibenclamide was identified by diode array detector,and the content determination was made by HPLC.Result:kuguasu Capsules was detecter to contain Glibencl... |
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| Keywords: | Traditional Chinese Medicine for health care kuguasu Capsules Glibenclamide TLC HPLC |
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