| 槐耳发酵液乙酸乙酯部位化学成分的研究 |
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| 引用本文： | 李可心,吕建华,董婧,范冬雨,王英平,李长田.槐耳发酵液乙酸乙酯部位化学成分的研究[J].中成药,2022(2):445-450. |
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| 作者姓名： | 李可心 吕建华 董婧 范冬雨 王英平 李长田 |
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| 作者单位： | 吉林农业大学食药用菌教育部工程研究中心;吉林农业大学人参新品种选育与开发国家地方联合工程研究中心 |
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| 基金项目： | 国家重点研发计划项目(2020YFD1000300)。 |
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| 摘 要： | 目的 探究槐耳Trames robiniophila Murrll.发酵液乙酸乙酯部位的化学成分.方法 槐耳发酵液乙酸乙酯部位采用硅胶、ODS、HPLC进行分离纯化,根据理化性质及波谱数据鉴定所得化合物的结构.结果 从中分离得到16个化合物,分别鉴定为尿嘧啶(1)、3,4-二羟基苯甲酸甲酯(2)、3,4-二羟基苯甲酸(...
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| 关 键 词： | 槐耳 发酵液 化学成分 分离鉴定 |
Chemical constituents from the ethyl acetate of fermentation liquid in Trames robiniophila |
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| LI Ke-xin,L Jian-hua,DONG jing,FAN Dong-yu,WANG Ying-ping,LI Chang-tian.Chemical constituents from the ethyl acetate of fermentation liquid in Trames robiniophila[J].Chinese Traditional Patent Medicine,2022(2):445-450. |
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| Authors: | LI Ke-xin L Jian-hua DONG jing FAN Dong-yu WANG Ying-ping LI Chang-tian |
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| Institution: | (Engineering Research Center of Chinese Ministry of Education for Edible and Medicinal Fungi,Jilin Agricultural University,Changchun 130118,China;National and Local Joint Engineering Research Center for Breeding and Development of New Ginseng varieties,Jilin Agricultural University,Changchun 130118,China) |
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| Abstract: | AIM To study the chemical constituents from the ethyl acetate of fermentation liquid in Trames robiniophila Murrll..METHODS The ethyl acetate of fermentation liquid in T.robiniophila was isolated and purified by silica,ODS and HPLC,then the structures of obtained compounds were identified by physicohemical properties and spectral data.RESULTS Sixteen compounds were isolated and identified as uracil(1),methyl 3,4-dihydroxybenzoate(2),3,4-dihydro-xybenzoicacid(3),1-phenyl-1,2-propanediol(4),cyclo(Leu-Pro)(5),cyclo(Phe-Ala)(6),cyclo(4-S-hydroxy-R-Pro-R-isoleucine),(7),cyclo(Phe-Gly)(8),cyclo(D-Hpro-L-Phe)(9),cyclo(L-Phe-L-Hpro)(10),methyl 4-hydroxybenzoate(11),p-hydroxybenzoicacid(12),p-hydroxybenzaldehyde(13),ethyl 3,4-dihydroxybenzoate(14),cyclo(Ala-lle)(15),cyclo(D-Leu-trans-4-hydroxy-L-Pro)(16).CONCLUSION All the compounds are isolated from the fungus fermentation liquid for the first time. |
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| Keywords: | Trames Robiniophila Murrll fermentation liquid chemical constituent isolation and identification |
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