| HPLC测定小金丸中乌头碱的含量 |
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| 引用本文： | 平欲晖,宗星星,关志宇,毛红梅. HPLC测定小金丸中乌头碱的含量[J]. 中国实验方剂学杂志, 2013, 19(9): 80-82 |
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| 作者姓名： | 平欲晖 宗星星 关志宇 毛红梅 |
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| 作者单位： | 江西中医学院,南昌,330004 |
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| 基金项目： | 国家重大新药创制项目项目(2009zx09310-005) |
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| 摘 要： | 目的:建立高效液相色谱法测定小金丸中乌头碱的含量.方法:采用ultimate C18柱(4.6 mm×250 mm,5 μm),以甲醇-0.03 mol·L-磷酸二氢钾溶液-三乙胺(45∶55∶0.04)为流动相,流速1.0 mL·min-,检测波长240 nm,柱温25℃.结果:乌头碱在0.114 ～2.28 μg具有良好的线性关系(r=0.999 8),平均回收率为97.79％,RSD 2.31％.结论:该方法准确、灵敏,重复性好,可用于小金丸中乌头碱的含量测定.
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| 关 键 词： | 小金丸 乌头碱 高效液相色谱 |
| 收稿时间： | 2011-11-02 |
HPLC Assaying of Aconitine in Xiaojin Pills |
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| PING Yu-hui,ZONG Xing-xing,GUAN Zhi-yu and MAO Hong-mei. HPLC Assaying of Aconitine in Xiaojin Pills[J]. China Journal of Experimental Traditional Medical Formulae, 2013, 19(9): 80-82 |
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| Authors: | PING Yu-hui ZONG Xing-xing GUAN Zhi-yu MAO Hong-mei |
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| Affiliation: | Department of Pharmacy, Jiangxi University of Traditional Chinese Medicine, Nanchang 330004, China;Department of Pharmacy, Jiangxi University of Traditional Chinese Medicine, Nanchang 330004, China;Department of Pharmacy, Jiangxi University of Traditional Chinese Medicine, Nanchang 330004, China;Department of Pharmacy, Jiangxi University of Traditional Chinese Medicine, Nanchang 330004, China |
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| Abstract: | |
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| Keywords: | Xiaojin pills aconitine HPLC |
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