| 填充柱气相色谱法测定蜂王浆中10-羟基-反-2-癸烯酸的含量 |
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| 引用本文： | 吉宁,于如嘏,杨清华,余品华,李颖. 填充柱气相色谱法测定蜂王浆中10-羟基-反-2-癸烯酸的含量[J]. 中国中药杂志, 1987, 12(9): 28-31 |
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| 作者姓名： | 吉宁 于如嘏 杨清华 余品华 李颖 |
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| 作者单位： | 中国药科大学分析化学教研室 |
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| 摘 要： | 本文应用填充柱气相色谱法对蜂王浆中10-羟基-反-2-癸烯酸含量进行了定量分析。将10-羟基-反-2-癸烯酸衍生化成甲酯衍生物,避免了硅烷化方法可能污染检测器的缺点。本文共测定了新鲜蜂王浆、蜂王浆冻干粉、蜂乳、人参蜂王浆、蜂乳胶囊、双宝素共七类样品中10-羟基-反-2-癸烯酸的含量。
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| 关 键 词： | 10-羟基-反-2-癸烯酸 蜂王浆 气相色谱 |
Determination of 10-Hydroxy-trans-2-Decenoic Acid (10-HDA) in Royal Jelly by Gas Liquid Chromatography |
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| Ji Ning,Yu Rugou: Yang Oinghua,Yu Pinhua and Li Ying. Determination of 10-Hydroxy-trans-2-Decenoic Acid (10-HDA) in Royal Jelly by Gas Liquid Chromatography[J]. China Journal of Chinese Materia Medica, 1987, 12(9): 28-31 |
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| Authors: | Ji Ning Yu Rugou: Yang Oinghua Yu Pinhua Li Ying |
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| Abstract: | A method for the quantitative determination of 10-HDA in royal jelly was established by liquid chromatography, with a packed column. The 10-HDA extracted with CH_2Cl_2 in a special extractor from royal jelly Could not be injected into the column directly. Methyl instead of silyl derivative of 10-HDA was used to circumvent the contamination of the detector. The method has successfully been applied to the determination of 10-HDA contents in raw royal jelly, granules, capsulae and tablets containing royal jelly. |
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| Keywords: | 10-hydroxy-trans-2-decenoic acid royal jelly gas liquid chromatography |
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