| 消毒液中过氧乙酸的气相色谱测定法 |
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| 引用本文： | 韩津生,孙文龙,袁爱红,刘香葵. 消毒液中过氧乙酸的气相色谱测定法[J]. 环境与健康杂志, 2004, 21(6): 410-411 |
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| 作者姓名： | 韩津生 孙文龙 袁爱红 刘香葵 |
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| 作者单位： | 天津市红桥区卫生防病站,天津,300132;天津市红桥区卫生防病站,天津,300132;天津市红桥区卫生防病站,天津,300132;天津市红桥区卫生防病站,天津,300132 |
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| 摘 要： | 目的建立消毒液中过氧乙酸的测定方法。方法采用FFAP色谱固定液和Chromosorb W-AW DMCS填充色谱柱，利用带氢火焰离子化检测器(FID)的气相色谱仪测定过氧乙酸。结果检出限为0．001％，线性范围0．01％。25％，回收率93％-102％，变异系数小于2．93％。结论该方法选择性强，灵敏度高，操作简便，分析速度快，样品不经分离可直接测定。
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| 关 键 词： | 色谱法 气相 消毒 过氧乙酸 |
| 文章编号： | 1001-5914(2004)06-0410-02 |
| 修稿时间： | 2003-10-21 |
Determination of Acetic Acid Peroxide in Disinfectant by Gas Chromatography |
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| HAN Jin-sheng,SUN Wen-long,YUAN Ai-hong,et al.. Determination of Acetic Acid Peroxide in Disinfectant by Gas Chromatography[J]. Journal of Environment and Health, 2004, 21(6): 410-411 |
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| Authors: | HAN Jin-sheng SUN Wen-long YUAN Ai-hong et al. |
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| Affiliation: | HAN Jin-sheng,SUN Wen-long,YUAN Ai-hong,et al.Sanitation and Anti-epidemic Station of Hongqiao District,Tianjin 300132,China |
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| Abstract: | Objective To established a method for determining the acetic acid peroxide in disinfectant. Methods The acetic acid peroxide determined by gas chromatography using FFAP fixative solution, Chromosorb W-AW DMCS column and FID detector. Results The detection limit was 0.001%.The linear range was from 0.01% to 25%.The recovery rate was 93%-102%?RSD was less than 2.93%. Conclusion The method is simple, rapid, sensitive and has a good selectivity. The sample can be directly detected without separation. |
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| Keywords: | Chromatography gas Disinfection Acetic acid peroxide |
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