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上标油指纹图谱的研究
引用本文:池浩波,赖怀恩,张梦虹,林晓辉.上标油指纹图谱的研究[J].海峡药学,2006,18(5):93-95.
作者姓名:池浩波  赖怀恩  张梦虹  林晓辉
作者单位:广东省潮州市药品检验所,潮州,521011;广东宏兴集团股份有限公司,潮州,5210011
摘    要:目的建立上标油色谱指纹图谱。方法应用毛细管气相色谱法,程序升温,并以萘为参照物.以相对保留时阍与相对峰面积为参数,建立10批样品的GC指纹图谱。结果标示出20个共有峰,其中主要峰的相对峰面积恒定。结论该法准确、精密度高、重现性好、可用于上标油的质量控制。

关 键 词:上标油  指纹图谱  CGS
文章编号:1006-3765(2006)05-0093-03

Study on Fingerprint of Siang Pure oil
CHI Hao-bo,LAI Huai-en,ZHANG Men-hong,LIN Xiao-hui.Study on Fingerprint of Siang Pure oil[J].Strait Pharmaceutical Journal,2006,18(5):93-95.
Authors:CHI Hao-bo  LAI Huai-en  ZHANG Men-hong  LIN Xiao-hui
Institution:Guangdong Chaozhou Institute for Drug Control, Chaozhou 521011, China ; 2. Guangdong Hongxing Group Co. Ltd. Chaozhou 521011, China
Abstract:OBJECTIVE To establish the CGC fingerprint of flavonoids in Siang Pure oil METHODS CGS fingerprint of ten samples were established with tetramethylsulphonium hydroxide,the naphthalene was used as internal standard,the relative migration time and the relative peak area were used as paramemeters. RESULTS 20 peaks occurred on the CGC fingerprint and the relative peak area was invariablenseCONCLUSION The method is accurate and precise with a good reproducibility,and it could be used for quality control of Siang Pure oil.
Keywords:Slang Pure oil  Fingerprint  CGC
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