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气相色谱法测定麝香跌打风湿膏中水杨酸甲酯的含量
引用本文:刘莉兰. 气相色谱法测定麝香跌打风湿膏中水杨酸甲酯的含量[J]. 中国现代药物应用, 2010, 4(16): 19-20
作者姓名:刘莉兰
作者单位:广东省食品药品职业技术学校教务科,510663
摘    要:目的建立测定麝香跌打风湿膏中水杨酸甲酯含量的方法。方法采用气相色谱法测定方中水杨酸甲酯的含量。结果水杨酸甲酯的线性范围为0.021796~1.0898mg.ml-1(r=0.99993);平均回收率为101.42%(RSD=2.9%,n=9)。结论本法操作简便、准确,专属性强,重复性好,能有效控制麝香跌打风湿膏的质量。

关 键 词:气相色谱法  麝香跌打风湿膏  水杨酸甲酯  含量测定

Analysis of Methyl salicylate in Shexiangdiedafengshi adhesive plaster by GC
LIU Li-lan. Analysis of Methyl salicylate in Shexiangdiedafengshi adhesive plaster by GC[J]. Chinese Journal of Modern Drug Application, 2010, 4(16): 19-20
Authors:LIU Li-lan
Affiliation:LIU Li-lan. Guangdong Food And Drug Vocational-technical School,Guangzhou 510663,China
Abstract:Objective To establish a method for determining the content of Methyl salicylate in Shexiangdiedafengshi adhesive plaster. Methods Methyl salicylate could be determined by GC. Results The linear range for Methyl salicylate was 0. 021796 ~ 1. 0898 mg/ml( r = 0. 99993) . The average recovery rate was 101. 42% ( RSD = 2. 9% ,n = 9) . Conclusion The method reported in this paper are easy to operate,which can provide accurate and reproducible results,and can be used for the quality control of Shexiangdiedafengshi adhesive plaster.
Keywords:GC  Shexiangdiedafengshi adhesive plaster  Methyl salicylate  Determination
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