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| 固相萃取小柱净化-气相色谱法测定蛴螬的有机氯农药残留 | |
| 引用本文： | 裴克,曹蔚,王发,杨倩,赵海峰,王四旺. 固相萃取小柱净化-气相色谱法测定蛴螬的有机氯农药残留[J]. 西北药学杂志, 2012, 27(1): 23-26. DOI: 10.3969/j.issn.1004-2407.2012.01.011 |
| 作者姓名： | 裴克 曹蔚 王发 杨倩 赵海峰 王四旺 |
| 作者单位： | 1. 陕西中医学院药学院,咸阳,712046 2. 第四军医大学药学系天然药物学教研室,西安,710032 3. 陕西省食品药品检验所,西安,710061 |
| 基金项目： | 陕西省食品药品监督管理局中药材标准课题(编号:2009003) |
| 摘 要： | 目的建立测定蛴螬中9种有机氯类农药残留量的方法。方法采用超声提取,固相萃取小柱净化,气相色谱法进行测定。结果所测定农药的回收率为84.0%～107.4%,样品中六六六的4种异构体、滴滴涕的4种异构体和五氯硝基苯的含量均符合国家的相关规定。结论该方法操作简便,灵敏,适用于蛴螬有机氯类农药的检测。 |
| 关 键 词： | 蛴螬 有机氯农药 气相色谱法 固相萃取 |
Determination of organochlorine pesticides in Holotrichia diomphalia using solid-phase extraction and gas chromatography |
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| PEI Ke,CAO Wei,WANG Fa,YANG Qian,ZHAO Haifeng,WANG Siwang. Determination of organochlorine pesticides in Holotrichia diomphalia using solid-phase extraction and gas chromatography[J]. Northwest Pharmaceutical Journal, 2012, 27(1): 23-26. DOI: 10.3969/j.issn.1004-2407.2012.01.011 | |
| Authors: | PEI Ke CAO Wei WANG Fa YANG Qian ZHAO Haifeng WANG Siwang |
| Affiliation: | 1.Medicine College of Shaanxi University of Chinese Medicine,Xianyang 712046,China;2.Department of Natural Medicine,School of Pharmacy,The Fourth Military Medical University,Xi’an 710032,China;3.Shaanxi Province Institute for Food and Drug Control,Xi’an 710061,China) |
| Abstract: | Objective To establish a method for the determination of the nine kinds of organochlorine pesticides in Holotrichia diomphalia.Methods The samples were extracted by ultrasonic wave,purified with solid-phase extraction column and determined by GC-ECD.Results For all of the analyzed pesticides,the recovery rates were in the range of 84.0%-107.4%,and the content of four isomers of BHC,four isomers of DDT and quintozene did not exceed the related national standards.Conclusion This method is simple,sensitive and can be applied to the detection of orthoptera organochlorine pesticides in Holotrichia diomphalia Bates. |
| Keywords: | Holotrichia diomphalia Bates organochlorine pesticides GC solid-phase extraction |
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