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当归含量测定时阿魏酸供试品制备条件的实验设计
引用本文:袁梦哲,李绍峰.当归含量测定时阿魏酸供试品制备条件的实验设计[J].河南中医药学刊,2010(1):120-121.
作者姓名:袁梦哲  李绍峰
作者单位:[1]周口市食品药品监督检验所,河南周口466000 [2]周口市环境监测站,河南周口466000
摘    要:目的:利用正交实验,研究当归中阿魏酸供试品制备的最佳条件。方法:利用药典检测方法,采用L9(34)正交实验表安排提取方法、药材形状、提取时间3个因素设计正交实验。结果:阿魏酸供试品制备的最佳方法为用极薄片超声波法提取20min。结论:用本实验方法制备供试品时间短,效率高,是制备阿魏酸供试品的最佳方法。

关 键 词:当归  阿魏酸  供试品制备  正交试验

The Experiment Design of Preparative Condition of Ferulaic Acid in Assaying Angelica Content
Yuan Mengzhe,Li Shaofeng.The Experiment Design of Preparative Condition of Ferulaic Acid in Assaying Angelica Content[J].Journal of Henan college of Traditional Chinese Medicine,2010(1):120-121.
Authors:Yuan Mengzhe  Li Shaofeng
Institution:1. Zhoukou Municipal Institute for Biochemical Drug Control,Zhoukou,Henan,China 4660002. Zhoukou Environmental Monitoring Station,Zhoukou,Henan,China 466000 )
Abstract:Objective:To explore the optimum condition in preparative condition of ferulaic acid in angelica by perpendicular experiment.Methods:The L9(34) was used to plan extraction,medicinal substances shape and extraction time and the dispensatory detected method was be used.Results:The optimum condition in preparative condition of ferulaic acid in angelica was extract 20 min by using thin slice and supersonic.Conclusion:Using this experiment method to preparative ferulaic acid was the optimum method for short time and efficient.
Keywords:angelica  ferulaic acid  trial preparation  perpendicular experiment
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