| 三七R胶囊质量标准研究 |
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| 引用本文： | 马妮,周家明,曾江,高明菊,朱琳,唐长国,崔秀明. 三七R胶囊质量标准研究[J]. 现代中药研究与实践, 2010, 0(5): 62-64 |
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| 作者姓名： | 马妮 周家明 曾江 高明菊 朱琳 唐长国 崔秀明 |
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| 作者单位： | [1]文山三七研究院新产品开发研究所,云南文山663000 [2]云南三七农业工程实验室,云南文山663000 [3]上海市静安区科学技术协会,上海200040 |
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| 摘 要： | 目的建立三七R胶囊的质量标准。方法采用HPLC法测定三七R胶囊中三七皂苷R1、人参皂苷Rg1及三七皂苷R2的含量。结果该法测定三七皂苷R1平均回收率为100.62%(RSD=2.99%,n=6);人参皂苷Rg1平均回收率为99.01%(RSD=1.91%,n=6);三七皂苷R2平均回收率为99.66%(RSD=2.38%,n=6)。结论本方法操作简便,结果可靠,准确,能有效地控制三七R胶囊的质量。
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| 关 键 词： | 三七R胶囊 质量标准 HPLC法 |
Study on Quality Standard for Sanqi R Granules |
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| Affiliation: | MA Ni,ZHOU Jia-ming,ZENG Jiang,Gao Ming-ju,Zhu Lin,Tang Chang-guo,CUI Xui-ming,(1.Wenshan Sanqi Research Institute,Wenshan 663000,China;2.Yunnan Sanqi Agricultural Engineering Laboratory,Wenshan 663000,China;3.Shanghai Jingan District Science and Technology of Association,Shanghai 200040,China) |
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| Abstract: | Objective To establish the quality standard for Sanqi R Granules.Methods The Shim-Pack C18（250 mm×4.6 mm,5 μm） column was used,with CH3CN-H2O gradually elutied and monitored was at 203 nm,determined the contents of notoginsenoside R1,ginsenoside Rg1 and notoginsenoside R2.Results The average recovery of notoginsenoside R1 was 100.62%（RSD=2.99%,n=6）.The average recovery of ginsenoside Rg1 was 99.01%（RSD= 1.91%,n= 6）.The average recovery of notoginsenoside R2 was 99.66%（RSD= 2.38%,n= 6）,the total contents limit of notoginsenoside R1,ginsenoside Rg1,notoginsenoside R2 shouldn,t be lower than 80 mg/tablet.Conclusion The method is simple,reliable,accurate and can be applied to the quality control of the Sanqi R Granules. |
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| Keywords: | Sanqi R Granules quality standard HPLC |
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