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| 养精种玉颗粒的定性定量方法研究 | |
| 引用本文： | 王婴,张婧,王岩,马红霞.养精种玉颗粒的定性定量方法研究[J].中国实验方剂学杂志,2013,19(15):76-78. |
| 作者姓名： | 王婴 张婧 王岩 马红霞 |
| 作者单位： | 1. 广东药学院医药化工学院,广东中山,528458 2. 广东药学院中药学院,广州,510006 3. 广州医学院第一附属医院,广州,510120 |
| 基金项目： | 国家自然科学基金项目(81273786); 广东省科技计划项目(粤科规划字[2011]97号); 中山市科技计划项目(2009H019) |
| 摘 要： | 目的:建立养精种玉颗粒的定性定量方法.方法:采用薄层色谱法对制剂中的白芍、当归、山茱萸进行鉴别；采用HPLC法测定芍药苷的含量.结果:薄层色谱斑点清晰,阴性对照无干扰；芍药苷进样量在60.56～605.6 ng与峰面积的线性关系良好(r=0.999 6),平均回收率99.2％ (RSD 1.5％).结论:建立的方法简便、准确、重复性好,可用于该制剂的质量控制. |
| 关 键 词： | 养精种玉颗粒 鉴别 含量测定 芍药苷 |
| 收稿时间： | 2012/10/2 0:00:00 |
Study on Qualitative and Quantitative Methods of Yangjingzhongyu Granules |
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| WANG Ying,ZHANG Jing,WANG Yan and MA Hong-xia.Study on Qualitative and Quantitative Methods of Yangjingzhongyu Granules[J].China Journal of Experimental Traditional Medical Formulae,2013,19(15):76-78. | |
| Authors: | WANG Ying ZHANG Jing WANG Yan and MA Hong-xia |
| Institution: | School of Chemistry and Chemical Engineering, Guangdong Pharmaceutical University, Zhongshan 528458, China;School of Traditional Chinese Medicine, Guangdong Pharmaceutical University, Guangzhou 510006, China;School of Traditional Chinese Medicine, Guangdong Pharmaceutical University, Guangzhou 510006, China;First Affiliated Hospital to Guangzhou Medical College, Guangzhou 510120, China |
| Abstract: | Objective: To establish the qualitative and quantitative methods for Yangjingzhongyu Granules. Method: Radix Paeoniae Alba, Angelica sinensis and Fructus corni in the preparation were identified by TLC, and the content of paeoniflorin was determined by HPLC. Result: The TLC spots were clear without interference of the other constituents in the preparation. The linear range of paeoniflorin was 60.56-605.6 ng (r=0.999 6). The average recovery was 99.2% (RSD 1.5%). Conclusion: The method is easy, accurate and reproducible. It can be used for quality control of the preparation. |
| Keywords: | Yangjingzhongyu Granules identification assay paeoniflorin |
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