| 电导率法在线监测栀子提取物大孔树脂柱分离工艺 |
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| 引用本文： | 张鹏,高峻峰,孟硕,刘建勋.电导率法在线监测栀子提取物大孔树脂柱分离工艺[J].中国实验方剂学杂志,2013,19(15):27-28. |
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| 作者姓名： | 张鹏 高峻峰 孟硕 刘建勋 |
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| 作者单位： | 中国中医科学院西苑医院实验研究中心,北京,100091 |
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| 基金项目： | 国家自然科学基金项目(30772755,81073060);国家科技重大专项(2009ZX09103-317) |
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| 摘 要： | 目的:利用电导法在线监测栀子提取液大孔树脂柱分离工艺.方法:利用电导计测定通过大孔树脂柱洗脱后流出成分的电导率变化,并考察其与去乙酰基车叶草苷酸甲酯、京尼平-1β-D龙胆双糖苷、栀子苷3个成分变化的相关性.结果:电导率先下降,之后随栀子等成分的被洗脱又明显升高,呈较好的相关性.结论:电导法可用于监测栀子提取物的大孔树脂分离工艺.
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| 关 键 词： | 大孔树脂 栀子 电导率 在线监测 去乙酰基车叶草苷酸甲酯 京尼平-1-β-D龙胆双糖苷 栀子苷 |
| 收稿时间： | 2012/11/27 0:00:00 |
Online Monitoring of Separation Technology with Macroporous Resin Column for Extract of Gardenia jasminoides by Conductivity Method |
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| ZHANG Peng,GAO Jun-feng,MENG Shuo and LIU Jian-xun.Online Monitoring of Separation Technology with Macroporous Resin Column for Extract of Gardenia jasminoides by Conductivity Method[J].China Journal of Experimental Traditional Medical Formulae,2013,19(15):27-28. |
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| Authors: | ZHANG Peng GAO Jun-feng MENG Shuo and LIU Jian-xun |
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| Institution: | Experimental Research Center, Xiyuan Hospital of China Academy of Chinese Medical Sciences, Beijing 100091, China;Experimental Research Center, Xiyuan Hospital of China Academy of Chinese Medical Sciences, Beijing 100091, China;Experimental Research Center, Xiyuan Hospital of China Academy of Chinese Medical Sciences, Beijing 100091, China;Experimental Research Center, Xiyuan Hospital of China Academy of Chinese Medical Sciences, Beijing 100091, China |
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| Abstract: | |
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| Keywords: | macroporous absorption resin Gardenia jasminoides conductivity online monitoring deacetyl-asperulosidic acid methyl ester genipin-1-β-D-gentiobioside geniposide |
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