| HPLC法测定竭红跌打贴膏剂中龙血素A和B的含量 |
| |
| 引用本文： | 白才堂,吕竹芬,邬威尧,谢清春,苏志伟,刘顺玲.HPLC法测定竭红跌打贴膏剂中龙血素A和B的含量[J].中国药师,2010,13(10):1465-1467. |
| |
| 作者姓名： | 白才堂 吕竹芬 邬威尧 谢清春 苏志伟 刘顺玲 |
| |
| 作者单位： | [1]广东省药物新剂型重点实验室／广东药学院药物研究所,广州510006 [2]佛山冯了性药业有限公司,广州510006 |
| |
| 基金项目： | 广东省佛山市产学研专项资金项目 |
| |
| 摘 要： | 目的：建立竭红跌打贴膏剂中龙血素A和B的含量测定方法。方法：采用高效液相色谱法，以十八烷基硅烷键合硅胶为固定相，甲醇-乙腈-0．05mol·L^-1磷酸二氢钾（31：13：56）为流动相，检测波长275nm，柱温35℃。结果：龙血素A在8．6369．00μg·ml^-1范围有良好线性关系（r=0．9999），平均回收率为98．59％；龙血素B在15．45。123．60μg·ml^-1范围有良好线性关系（r=0．9999），方法平均回收率为98．46％。结论：本方法可测定竭红跌打贴膏剂中龙血素A和B含量，结果准确、可行。
|
| 关 键 词： | 竭红跌打贴膏剂 龙血素A 龙血素B |
Determination of Loureirin A and B in Jiehong Dieda Adhesive Ointment by HPLC |
| |
| Bai Caitang,Lv Zhufen,Wu Weiyao,Xie Qingchun,Su Zhiwei,Liu Shunling.Determination of Loureirin A and B in Jiehong Dieda Adhesive Ointment by HPLC[J].China Pharmacist,2010,13(10):1465-1467. |
| |
| Authors: | Bai Caitang Lv Zhufen Wu Weiyao Xie Qingchun Su Zhiwei Liu Shunling |
| |
| Institution: | 1. Key laboratory of Advanced Drug Delivery of Guangdong Province ,Institute of Material Medica, Guangdong College of Pharmacy, Guangzhou 510006, China ;2. Foshan Fengliaoxing Pharmaceutical Co. , Ltd. ) |
| |
| Abstract: | Objective： To establish a method for determination of loureirin A and B in jiehong dieda adhesive ointment. Method： The C18 column was used,methanol-acetonitril-0. 05 mol ·L^-1 potassium dihydrogen phosphate （31： 13： 56） was used for mobile phase and detective wavelength was set at 275 nm. The column temperature was 35 ℃. Result： The standard curves of loureirin A was linear within the concentration range of 8. 63-69. 00 μg· ml ^-1 （r = 0. 999 9 ）. The average recovery was 98.59%. The standard curves of loureirin B was linear within the concentration range of 15.45-123.60μg· ml ^-1 （r =0. 999 9）. The average recovery was 98. 46%. Conclusion： The assaying method is accurate and reliable for determination of loureirin A and loureirin B in jiehong dieda adhesive ointment. |
| |
| Keywords: | Jiehongdieda adhesive ointment Loureirin A Loureirin B |
| 本文献已被 维普 万方数据 等数据库收录！ |
|
