| 高效液相色谱法同时鉴定保健品中非法添加的四种降糖药成分 |
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| 引用本文： | 曾茂法,张学斌. 高效液相色谱法同时鉴定保健品中非法添加的四种降糖药成分[J]. 中国现代应用药学, 2006, 23(6): 506-507 |
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| 作者姓名： | 曾茂法 张学斌 |
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| 作者单位： | 浙江省台州市药品检验所,浙江,台州,318000 |
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| 摘 要： | 目的建立高效液相色谱法同时鉴定保健品中非法添加的四种降糖药成分。方法色谱条件1:Symm etry-C18柱、流动相为甲醇-水(含十二烷基硫酸钠0.03%与三乙胺0.1%,调节pH值至3.5)(67∶33),流速为1.0mL.m in-1;DAD检测器,检测波长234nm;色谱条件2:Zorbax-C8柱,其余同色谱条件1。利用提取的色谱与光谱鉴定。结果格列本脲、盐酸苯乙双胍、盐酸二甲双胍、甲苯磺丁脲等四种成分得到分离并鉴定。结论该方法简便可靠,可一次鉴定是否含上述四种成分。
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| 关 键 词： | 高效液相色谱法 保健品 降糖药成分 鉴定 |
| 文章编号： | 1007-7693（2006）06-0506-02 |
| 收稿时间： | 2005-06-21 |
| 修稿时间： | 2005-06-21 |
Identification of four components of diabetes medicine added illegally to health products by HPLC |
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| ZENG Mao-f,ZHANG Xue-bin. Identification of four components of diabetes medicine added illegally to health products by HPLC[J]. The Chinese Journal of Modern Applied Pharmacy, 2006, 23(6): 506-507 |
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| Authors: | ZENG Mao-f ZHANG Xue-bin |
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| Abstract: | OBJECTIVE To establish a method for identification of four components of diabetes medicine added illegally to health products by HPLC.METHODS It was conducted with two chromatographic conditions.The condition 1: Symmetry-C18 column was used with the mobil |
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| Keywords: | HPLC health products components of diabetes medicine identification |
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