| 保肾灵胶囊质量标准研究 |
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| 引用本文： | 孙成荣,张娴,康阿龙,李书桐,张锁成,郭超.保肾灵胶囊质量标准研究[J].中国药房,2009(12):928-930. |
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| 作者姓名： | 孙成荣 张娴 康阿龙 李书桐 张锁成 郭超 |
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| 作者单位： | 解放军第451医院,西安市710054 |
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| 摘 要： | 目的:建立保肾灵胶囊的质量标准。方法:采用薄层色谱(TLC)法对方中黄芪、大黄、川芎、水蛭进行定性鉴别;采用高效液相色谱法测定该制剂中二苯乙烯苷的含量。结果:TLC中能准确鉴别出黄芪、大黄、川芎、水蛭的特征斑点。二苯乙烯苷的进样量在0.176～0.880μg范围内与峰面积积分值呈良好线性关系(r=0.999 8);平均回收率为98.9%,RSD=1.3%(n=6)。结论:所建标准可用于保肾灵胶囊的质量控制。
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| 关 键 词： | 保肾灵胶囊 薄层色谱法 高效液相色谱法 质量标准 |
Quality Standard of Baoshenling Capsules |
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| SUN Cheng-rong,ZHANG Xian,KANG A-long,LI Shu-tong,ZHANG Suo-cheng,GUO Chao.Quality Standard of Baoshenling Capsules[J].China Pharmacy,2009(12):928-930. |
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| Authors: | SUN Cheng-rong ZHANG Xian KANG A-long LI Shu-tong ZHANG Suo-cheng GUO Chao |
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| Institution: | (No. 451 Hospital of PLA, Xi＇an 710054, China) |
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| Abstract: | OBJECTIVE： To establish the quality standard of Baoshenling capsules. METHODS： Radix Astragali, Radix et Rhizoma Rhei, Ligusticum chuanxiong and Hirudo were identified qualitatively by TLC, and the content of diphenyl ethylene in Baoshenling capsules was determined by HPLC. RESULTS： The characteristic TLC spots of Radix Astragali, Radix et Rhizoma Rhei, Ligusticum chuanxiong and Hirudo were identified accurately. The linear range of diphenyl ethylene was 0.176- 0. 880μg（ r = 0.999 8） with an average recovery rate of 98.9% （RSD = 1.3%, n = 6） . CONCLUSION ： The established standard is applicable for the quality control of Baoshenling capsules. |
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| Keywords: | Baoshenling capsules TLC HPLC Quality standard |
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