| 滴鼻灵质量标准研究 |
| |
| 引用本文： | 吴钉红,陈燕芬,朱尚虹.滴鼻灵质量标准研究[J].中国药房,2009(12):926-927. |
| |
| 作者姓名： | 吴钉红 陈燕芬 朱尚虹 |
| |
| 作者单位： | 广东省中医院,广州市510120 |
| |
| 摘 要： | 目的:建立滴鼻灵的质量标准。方法:采用薄层色谱(TLC)法对方中黄连进行定性鉴别;采用反相高效液相色谱法测定该制剂中盐酸麻黄碱的含量。结果:TLC中斑点清晰、分离度好。盐酸麻黄碱的进样量在0.088～3.520μg范围内与峰面积积分值呈良好线性关系(r=0.996 0);平均回收率为100.82%,RSD=1.19%(n=6)。结论:所建标准可用于滴鼻灵的质量控制。
|
| 关 键 词： | 滴鼻灵 薄层色谱法 高效液相色谱法 质量标准 |
Quality Standard of Dibiling |
| |
| WU Ding-hong,CHEN Yan-fen,ZHU Shang-hong.Quality Standard of Dibiling[J].China Pharmacy,2009(12):926-927. |
| |
| Authors: | WU Ding-hong CHEN Yan-fen ZHU Shang-hong |
| |
| Institution: | (Guangdong Provincial Hospital of TCM, Guangzhou 510120, China) |
| |
| Abstract: | OBJECTIVE： To establish the quality standard of Dibiling. METHODS： Rhizoma Coptidis in the formulation was identified qualitatively by TLC, and the content of ephedrine hydrochloride was determined by RPHPLC. RESULTS： The TLC spots of Rhizoma Coptidis were cJear and distinctive. The linear range of ephedrine hydroehloride was 0.088-3. 520 μg（ r= 0.996 0） with an average recovery rate of 100.82% （RSD = 1.19%, n = 6） .CONCLUSION ： The established standard is applicable for the quality control of Dibiling. |
| |
| Keywords: | Dibiling TLC HPLC Quality standard |
| 本文献已被 维普 等数据库收录！ |
