| 高效液相色谱法测定妇炎康丸中芍药苷的含量 |
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| 引用本文： | 邹玉繁,汪小根. 高效液相色谱法测定妇炎康丸中芍药苷的含量[J]. 现代医药卫生, 2009, 25(9): 1304-1305 |
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| 作者姓名： | 邹玉繁 汪小根 |
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| 作者单位： | 邹玉繁 (广东食品药品职业学院,广东,广州,510520)； 汪小根 (广东食品药品职业学院,广东,广州,510520)； |
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| 摘 要： | 目的：观察高效液相色谱法（HPLC）测定妇炎康丸中芍药苷的含量。方法：采用Diaminsil C18 ODS（5μm，4．6×200mm），以乙腈-0．05mol/L磷酸二氢钾溶液（14：86）为流动相，紫外检测波长为230nm。结果：芍药苷在0．304～1．216μg范围内呈良好的线性关系（r=0．9997），平均回收率为99．5％（n=9），RSD分别为1．05％。结论：本方法准确、可靠、重现性好，可适用于妇炎康丸中芍药苷的含量测定。
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| 关 键 词： | 妇炎康丸 芍药苷 高效液相色谱法 含量测定 |
Determination of paeoniflorin in Fuyankang Pills by HPLC |
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| ZOU Yu-fan,WANG Xiao-gen. Determination of paeoniflorin in Fuyankang Pills by HPLC[J]. JOURNAL OF MODERN MEDICINE & HEALTH, 2009, 25(9): 1304-1305 |
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| Authors: | ZOU Yu-fan WANG Xiao-gen |
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| Affiliation: | ( Guangdong Food and Drug Vocational College ,Guangzhou,Guangdong 510520,China) |
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| Abstract: | Objective：To establish a method for the determination of paeoniflorin in Fuyankang Pills by HPLC. Methods：The HPLC method was performed on a Diaminsil C18 ODS column （5μm,4.6×200mm,the composition of mobile phase was acetonitrile-0.05% potassium phosphate monobasic solution （14：86）,the wavelength was 230nm. Results：The linear range of paeonitlorin was 0.304-1.216 μg （r=0.9997）. The average recovery rate of paeoniflorin was 99.5 % with RSD of 1.05%. Conclusion：This method is accurate, reliable and reproducible. It can be used for assaying of paeoniflorin in Fuyankang Pills. |
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| Keywords: | Fuyankang Pills Paeoniflorin HPLC Content determination |
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