| HPLC法测定桂丹莪棱口服液中芍药苷的含量 |
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| 引用本文： | 邓松岳,王伟丽,朱明伟,杨文文.HPLC法测定桂丹莪棱口服液中芍药苷的含量[J].中国医药导报,2012,9(10):139-140. |
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| 作者姓名： | 邓松岳 王伟丽 朱明伟 杨文文 |
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| 作者单位： | 1. 河南省商丘市食品药品检验所,河南商丘,476000
2. 天津天狮集团有限公司,天津,301700 |
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| 摘 要： | 目的建立桂丹莪棱口服液的质量标准。方法采用HPLC法对桂丹莪棱口服液中芍药苷的含量进行测定。结果桂丹莪棱口服液中芍药苷的含量在0.308 2～6.164 0μg的范围内,有良好的线性关系,r=0.999 9,平均回收率为98.68%,RSD=1.01%,桂丹莪棱口服液中芍药苷的含量为1.392 mg/mL。结论建立了桂丹莪棱口服液的质量标准,该方法操作易行,稳定可靠,可用于桂丹莪棱口服液中芍药苷的含量及该制剂的质量控制。
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| 关 键 词： | 桂丹莪棱口服液 芍药苷 高效液相色谱法 |
Contents determination of Paeoniflori in Guidan′eleng Mixture by HPLC |
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| DENG Songyue
,
WANG Weili
,
ZHU Mingwei
,
YANG Wenwen.Contents determination of Paeoniflori in Guidan′eleng Mixture by HPLC[J].China Medical Herald,2012,9(10):139-140. |
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| Authors: | DENG Songyue WANG Weili ZHU Mingwei YANG Wenwen |
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| Institution: | 1.Shangqiu Institute for Food and Drug Control,He′nan Province,Shangqiu 476000,China;2.Tianjin Tiens Group Co.Ltd,Tianjin 301700,China |
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| Abstract: | Objective To establish the standard for determination of Paeoniflori in Guidan′eleng Mixture.Methods Paeoniflori in Guidan′eleng Mixture were determined by HPLC.Results The linear range of Paeoniflori was 0.308 2-6.164 0 μg,r = 0.999 9.The average recovery of Paeoniflori was 98.68% and RSD was 1.01%.Contents determination of Paeoniflori in Guidan′eleng Mixture was 1.392 mg/mL.Conclusion The method is simple,sensitive and accurte,and can be used to determine Paeoniflori and as the quality control of Guidan′eleng Mixture. |
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| Keywords: | Guidan′eleng Mixture Paeoniflori HPLC |
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