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麻甘合剂的质量标准
引用本文:黄国军,李湘玲,易淼,舒跃生. 麻甘合剂的质量标准[J]. 中国医院药学杂志, 2001, 21(3): 155-157
作者姓名:黄国军  李湘玲  易淼  舒跃生
作者单位:湖北省妇幼保健院,湖北 武汉 430070
摘    要:目的:研究麻甘合剂的质量标准,建立杏仁、甘草的薄层色谱法(TLC)和盐酸麻黄碱的高效液相色谱法(HPLC)。方法:流动相为乙膊-三乙胺-磷酸-水(1.8:0.1:0.1:9.8),检测波长为214nm,样品提取过滤后进行分析。结果:线性范围20-200ug.ml^-1相关系数r=0.9996,精密度为1.20%,加样回收率100.34%。结论:该方法适用于麻甘合剂的质量控制。

关 键 词:麻甘合剂 薄层色谱法 高效液相色谱法 中药 质量标准
文章编号:1001-5213(2001)03-0155-03
修稿时间:1999-07-16

Study on the qualitystandards for mistura magan
HUANG Guo-Jun,LI Xiang-Ling,YI Miao,et al. Study on the qualitystandards for mistura magan[J]. Chinese Journal of Hospital Pharmacy, 2001, 21(3): 155-157
Authors:HUANG Guo-Jun  LI Xiang-Ling  YI Miao  et al
Abstract:OBJECTIVE:The quality standards for mistura magan have beenstudied.The TLC methods for prunus armeniaca and Glycyrrhiza uralensis were established.A simple high performance liquid chromatographic method was established for determination of Ephedrine Hydrochloride.METHODS:The mobile phase was acetonitrile-triethylammine-phosphoric acid-water(1.8∶0.1∶0.1∶9.8).The UV dectector was set at 214nm.The sample was extracted by mobile phase.RESULTS:The linear range was from 20~200 μg.ml-1,r=0.9996.The relative standard deviation was 1.20%.The recovery was 100.34%.CONCLUSIONS:The method is suitable for the quality standards of mistura magan.
Keywords:mistura magan  TLC  HPLC  
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