| 硫酸铁铵催化合成乙酰乙酸乙酯乙二醇缩酮 |
| |
| 引用本文： | 丁盈红,谭莉萍. 硫酸铁铵催化合成乙酰乙酸乙酯乙二醇缩酮[J]. 广东药学院学报, 2002, 18(2): 81-82 |
| |
| 作者姓名： | 丁盈红 谭莉萍 |
| |
| 作者单位： | 广东药学院有机化学教研室,广东广州,510224;广东药学院有机化学教研室,广东广州,510224 |
| |
| 摘 要： | 采用正交试验优选出最佳条件为：当乙酰乙酸乙酯为0.2moL时,硫酸铁铵0.7g,环乙烷10mL。乙酰乙酸乙酯和惭二醇摩尔比为1：1.5,反应时间为5h。所得产率为59.2%。
|
| 关 键 词： | 硫酸铁铵 乙酰乙酸乙酯乙二醇缩酮 正交试验 |
| 文章编号： | 1006-8783(2002)02-0081-02 |
| 修稿时间： | 2002-04-26 |
Catalytic synthesis of ethyl acetoacetate ethylene glycol ketal by ammonium ferric sulfate |
| |
| DING Ying hong,TAN Li ping. Catalytic synthesis of ethyl acetoacetate ethylene glycol ketal by ammonium ferric sulfate[J]. Academic Journal of Guangdong College of Pharmacy, 2002, 18(2): 81-82 |
| |
| Authors: | DING Ying hong TAN Li ping |
| |
| Abstract: | Ethyl acetoacetate ethylene glycol ketal (Fructon) was synthesized by reaction of ethyl acetoacetate and ethylene glycol using ammonium ferric sulfate as a catalyst. The optimum reation conditions were established through orthogonal test. |
| |
| Keywords: | ammonium ferric sulfate ethyl acetoacetate ethylene glycol ketal orthogonal test |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
