| 山奈酚-锰配合物的化学合成 |
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| 引用本文： | 徐芳芳,齐学洁,张毅,赵培莉,鞠辉.山奈酚-锰配合物的化学合成[J].辽宁中医学院学报,2011(7):226-227. |
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| 作者姓名： | 徐芳芳 齐学洁 张毅 赵培莉 鞠辉 |
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| 作者单位： | 天津中医药大学中药化学与分析重点实验室,天津300193 |
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| 基金项目： | 天津中医药大学中药学院本科生创新基金资助项目（200812） |
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| 摘 要： | 目的：探讨山奈酚与锰的反应条件并合成山奈酚锰配合物。方法：采用正交实验方法确定配合反应的最佳酸度、原料的物质的量比、温度、反应时间。结果：反应时间对产率的影响显著，原料物质的量比次之，pH影响最小。结论：山奈酚与氯化锰的物质的量比为1．0：2．5，pH为6，25℃下反应3h配合物的产率最大。且经紫外、红外光谱测定推测其结构。
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| 关 键 词： | 山奈酚 配合物 合成 |
Chemical Synthesis of Kaempferol and Manganese Complex |
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| XU Fang-fang,QI Xue-jie,ZHANG Yi,ZHAO Pei-li,JU Hui.Chemical Synthesis of Kaempferol and Manganese Complex[J].Journal of Liaoning College of Traditional Chinese Medicine,2011(7):226-227. |
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| Authors: | XU Fang-fang QI Xue-jie ZHANG Yi ZHAO Pei-li JU Hui |
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| Institution: | ( Traditional Chinese Medical Chemistry Analysis Key Laboratories, Tianjin University of Traditional Chinese Medicine, Tianjin 300193, China ) |
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| Abstract: | Objective ： To investigate the best conditions of the chemical reaction between kaempferol and manganese and to get kaempferol and manganese complex. Methods ： By single factor experiment for foundation, using the orthogonal experiment method to determine the best reaction pH, the molar ratio of raw materials, reaction temperature and reaction time. Results ： Reaction time had most significant effect, amount of substance had less effect, pH had lest effect on the yield. Conclusion ： Chemical synthesis of kaempferol and manganese has been tested to be at maximum with amount of substance ： 1.0 ： 2.5, pH 6, temperature at 25 ℃ , reaction time for 3h. The complex has been characterized by spectrum methods. |
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| Keywords: | kaempferol complexes synthesis |
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