| 东田糖脉灵颗粒质量标准研究 |
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| 引用本文： | 唐雪梅.东田糖脉灵颗粒质量标准研究[J].辽宁中医学院学报,2011(7):223-225. |
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| 作者姓名： | 唐雪梅 |
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| 作者单位： | 四川省第四人民医院,四川成都610016 |
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| 摘 要： | 目的：制定东田糖脉灵颗粒（黄连、红芪、生地、黄芩、姜黄）的质量标准。方法：用薄层色谱法鉴别黄连和黄芩；用高效液相色谱法测定盐酸小檗碱的含量。结果：盐酸小檗碱在0．2-4μg范围内呈良好的线形关系，r=0．9999，平均回收率为98．99％，RSD=1．76％。结论：鉴别方法专属性强，定量方法简便、准确可靠，可用于该制剂的质量控制。
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| 关 键 词： | 东田糖脉灵颗粒 盐酸小檗碱 黄芩苷 TLC HPLC |
Quality Standard for Dongtian Tangmai Ling Granules |
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| TANG Xue-mei.Quality Standard for Dongtian Tangmai Ling Granules[J].Journal of Liaoning College of Traditional Chinese Medicine,2011(7):223-225. |
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| Authors: | TANG Xue-mei |
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| Institution: | TANG Xue-mei ( Fourth People＇s Hospital of Sichuan Province, Chengdu 610016, Sichuan, China ) |
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| Abstract: | Objective ： To establish the quality control of Dongtian Tangmai Ling Granules （ Rhizoma Coptidis, Radix Hedysari, Radix Scutellariae, Rhizoma Curcumae Longae ）. Methods：Rhizoma Coptidis, Radix Scutellariae in Dongtian Tangmai Ling Granules weue identified by TLC.The content of flumazenil and injection in Dongtian Tangmai Ling Granules were determined by RP-HPLC. Results ： Flumazenil and injection showed a good relationship at a range of 0.2-0.4 μg （ r=0.9999 ） .The average recovery of flumazenil and injection in Dongtian Tangmai Ling Granules was 98.99% and RSD was 1.76%. Conclusion ： The method is simple, specific and accurate. The study provide a method for the quality control of Dongtiantangmailing Granules. |
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| Keywords: | Dongtian Tangmai Ling Flumazenil Baicalin TLC HPLC |
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