| 气相色谱法测定心力丸中麝香酮的含量 |
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| 引用本文： | 张电光,曾凡,吴冬玲. 气相色谱法测定心力丸中麝香酮的含量[J]. 广东药学院学报, 2009, 25(1): 31-33 |
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| 作者姓名： | 张电光 曾凡 吴冬玲 |
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| 作者单位： | 广东省药物研究所,广东广州,510440;广东省药物研究所,广东广州,510440;广东省药物研究所,广东广州,510440 |
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| 基金项目： | 广东省中医药管理局立项资助课题 |
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| 摘 要： | 目的建立心力丸中麝香酮含量的测定方法。方法采用SPBTM-1FUSED SILICA Capillary Column（30 m×0.32 mm×1.0μm）毛细管柱,火焰离子化检测器（FID）,以N2为载气,柱温：200℃,进样口温度：210℃,检测器温度：225℃。结果麝香酮在0.076-1.5 mg·mL^-1的范围内与其峰面积呈良好线性关系（r=0.999 6）,麝香酮的平均回收率为99.5%（n=9）,RSD为1.64%。结论本法简便、准确,可用于控制该制剂的质量。
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| 关 键 词： | 气相色谱法 心力丸 麝香酮 |
Content analysis of muscone in Xinli pills by gas chromatography |
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| ZHANG Dian-guang,ZENG Fan,WU Dong-ling. Content analysis of muscone in Xinli pills by gas chromatography[J]. Academic Journal of Guangdong College of Pharmacy, 2009, 25(1): 31-33 |
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| Authors: | ZHANG Dian-guang ZENG Fan WU Dong-ling |
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| Affiliation: | ZHANG Dian-guang,ZENG Fan,WU Dong-ling(Guangdong Institute of Drug Research,Guangzhou,Guangdong 510440,China) |
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| Abstract: | Objective To establish a method for analyzing the content of muscone in Xinli pills. Methods Samples were analyzed on a silica capillary column （30 m×0. 32 mm, 1.0 μm） using FID as detector andnitrogen as gas carrier. The column temperature, injector temperature and detector temperature were 200 ℃, 210 ℃ and 225 ℃, respectively. Results Muscone showed good linearity over the range of 0. 076 -1.5 mg · mL^-1 （r =0. 999 6）. The average recovery was 99.5% with RSD of 1.64% （n = 9）. Conclusion The method is simple and accurate for the quality control of the pills. |
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| Keywords: | muscone Xinli pills gas chromatography |
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