| 活血膏薄层鉴别及乌头碱限量检查 |
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| 引用本文： | 刘鹿岩. 活血膏薄层鉴别及乌头碱限量检查[J]. 实用中医内科杂志, 2011, 25(4): 108-108. DOI: 10.3969/j.issn.1671-7813.2011.04.61 |
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| 作者姓名： | 刘鹿岩 |
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| 作者单位： | 辽宁省本溪市中医院,辽宁本溪,117000 |
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| 摘 要： | [目的]研究活血膏的质量标准。[方法]采用TLC法对制剂中续断进行了定性鉴别实验,应用TLC法对制剂中主药生草乌的有效成分乌头碱进行了限量试验。[结果]薄层色谱中样品色谱斑点显色清晰,分离度好。乌头碱限量检查同样杂质干扰小、分离度好。[结论]本法灵敏、准确,专属性强,重现性好,可作为该制剂的质量控制方法。
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| 关 键 词： | 活血膏 TLC 乌头碱限量 质量标准 |
Huoxue Paste TLC Identification and Aconitine Limit Test |
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| LIU Lu-yan. Huoxue Paste TLC Identification and Aconitine Limit Test[J]. , 2011, 25(4): 108-108. DOI: 10.3969/j.issn.1671-7813.2011.04.61 |
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| Authors: | LIU Lu-yan |
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| Affiliation: | LIU Lu-yan(Traditional Chinese Medicine Hospital of Benxi,Benxi 117000,Liaoning,China) |
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| Abstract: | [Objective]Research the Huoxue Paste quality standards.[Method]TLC method of preparation for the qualitative identification of Dipsacus experiment,application of TLC method of main ingredients of formulations the active ingredient in Radix Health conducted a limited test of aconitine.[Results]TLC spots in the sample color clear chromatographic separation is good.Aconitine impurity limit test of the same small,separation is good.[Conclusion]The method is sensitive,accurate,specific,reproducible,and can be used for thequality control methods. |
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| Keywords: | TLC |
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