| 血府逐瘀口服液中芍药苷含量的测定 |
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| 引用本文： | 陈华,姜云平,高朝霞,吴东,江红丽.血府逐瘀口服液中芍药苷含量的测定[J].西部医学,2009,21(12):2162-2163. |
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| 作者姓名： | 陈华 姜云平 高朝霞 吴东 江红丽 |
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| 作者单位： | 成都军区总医院药剂科,四川成都,610083 |
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| 摘 要： | 目的建立血府逐瘀口服液中芍药苷含量测定的方法。方法用RP—HPLC法测定血府逐瘀口服液中芍药苷的含量，固定相为ZORBAXSB-C18柱（4．6×250mm，5μm）；流动相为乙腈：甲醇：1％冰醋酸（5：24：71）；流速：1．0ml／min；柱温：25℃；检测波长：240nm。结果芍药苷含量测定的线性范围是0．3847．68vg，r＝0．9998，平均加样回收率是101．96％，RSD＝3．77％。结论该方法简便易行，结果准确，可用于血府逐瘀口服液中芍药苷的含量测定。
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| 关 键 词： | 血府逐瘀口服液 芍药苷 反相高效液相色谱法 |
Detecting peoniflorin in Xuefuzhuyu liquor |
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| Institution: | CHENG Hua,JIANG Yun-ping, GAO Zhao-xia, et al (Department of Pharmacy, The General Hospital of Chengdu Military Area of PLA, Chengdu 610083,China) |
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| Abstract: | Objective To set up an antiphase high performance liquid chromatography for determination of peoniflorin in Xuefuzhuyu liquor. Methods The condition of determination was optimized. The static phase was C18（5μm,4. 6 × 250mm）and mobile phase was acetonitrile-methanol-1% glacial acetic acid（5：24： 71）that was used at 25℃ with a flow rate of 1.0 ml. min-1. The detection wavelength was 240nm. Results The liaearity, coefficient and the average recovery were 0. 384-7.68μg , 0. 9998 and 101.96%, respectively. Conclusion This is a simple and accurate detection method for the quality control of peoniflorin in Xuefuzhuyu liquor. |
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| Keywords: | Xuefuzhuyu liquor Peoniflorin RP-HPLC |
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