| HPLC法测定稳心颗粒中三七皂苷R_1、人参皂苷Rg_1、Rb_1、Rd与党参炔苷的含量 |
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| 引用本文： | 南国,张鹏,王萌,王跃飞,朱彦,吴红华.HPLC法测定稳心颗粒中三七皂苷R_1、人参皂苷Rg_1、Rb_1、Rd与党参炔苷的含量[J].天津中医药,2016,33(7):434-436. |
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| 作者姓名： | 南国 张鹏 王萌 王跃飞 朱彦 吴红华 |
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| 作者单位： | 天津中医药大学, 天津市现代中药重点实验室, 天津 300193;天津国际生物医药联合研究院中药新药研发中心, 天津 300457,天津中医药大学, 天津市现代中药重点实验室, 天津 300193;天津国际生物医药联合研究院中药新药研发中心, 天津 300457,天津中医药大学, 天津市现代中药重点实验室, 天津 300193;天津国际生物医药联合研究院中药新药研发中心, 天津 300457,天津中医药大学, 天津市现代中药重点实验室, 天津 300193;天津国际生物医药联合研究院中药新药研发中心, 天津 300457,天津中医药大学, 天津市现代中药重点实验室, 天津 300193;天津国际生物医药联合研究院中药新药研发中心, 天津 300457,天津中医药大学, 天津市现代中药重点实验室, 天津 300193;天津国际生物医药联合研究院中药新药研发中心, 天津 300457 |
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| 基金项目： | 科技部国际国家合作专项（2013DFA31620）。 |
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| 摘 要： | 目的]建立高效液相法(HPLC)同时测定稳心颗粒中三七皂苷R_1、人参皂苷Rg_1、Rb_1、Rd与党参炔苷的含量。方法]采用Agilent1260 DAD高效液相色谱仪,Amethyst C18色谱柱(4.6 mm×250 mm,4μm),乙腈-水为流动相,检测波长为210 nm,流速1 m L/min。结果]三七皂苷R1对照品在8~247 mg/L线性关系良好,平均回收率为102.69%,RSD=2.74%(n=6);人参皂苷Rg_1对照品在14~422 mg/L线性关系良好,平均回收率为98.72%,RSD=1.85%(n=6);党参炔苷对照品在1.5~42 mg/L线性关系良好,平均回收率为97.69%,RSD=1.94%(n=6);人参皂苷Rb_1对照品在2.65~847 mg/L线性关系良好,回收率为102.11%,RSD=1.96%(n=6);人参皂苷Rd对照品在8~255 mg/L线性关系良好,平均回收率为99.66%,RSD=2.49%(n=6)。结论]本实验中三七皂苷R_1、人参皂苷Rg_1、Rb_1、Rd和党参炔苷的含量测定方法稳定可靠,可作为稳心颗粒中三七皂苷R1、人参皂苷Rg_1、Rb_1、Rd与党参炔苷含量测定方法。
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| 关 键 词： | 稳心颗粒 高效液相色谱法 三七皂苷R1 人参皂苷Rg1 党参炔苷 人参皂苷Rb1 人参皂苷Rd |
| 收稿时间： | 2016/1/12 0:00:00 |
Determination of Notoginsenoside R1, Ginsenoside Rg1, Rb1, Rd and Lobetyolin in Wenxin Keli by HPLC |
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| NAN Guo,ZHANG Peng,WANG Meng,WANG Yue-fei,ZHU Yan and WU Hong-hua.Determination of Notoginsenoside R1, Ginsenoside Rg1, Rb1, Rd and Lobetyolin in Wenxin Keli by HPLC[J].Tianjin Journal of Traditional Chin Medicine,2016,33(7):434-436. |
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| Authors: | NAN Guo ZHANG Peng WANG Meng WANG Yue-fei ZHU Yan and WU Hong-hua |
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| Institution: | Tianjin State Key Laboratory of Modern Chinese Medicine, Tianjin University of Traditional Chinese Medicine, Tianjin 300193, China;Research and Development Center of Traditional Chinese Medicine, Tianjin International Joint Academy of Biotechnology and Medicine, Tianjin 300457, China,Tianjin State Key Laboratory of Modern Chinese Medicine, Tianjin University of Traditional Chinese Medicine, Tianjin 300193, China;Research and Development Center of Traditional Chinese Medicine, Tianjin International Joint Academy of Biotechnology and Medicine, Tianjin 300457, China,Tianjin State Key Laboratory of Modern Chinese Medicine, Tianjin University of Traditional Chinese Medicine, Tianjin 300193, China;Research and Development Center of Traditional Chinese Medicine, Tianjin International Joint Academy of Biotechnology and Medicine, Tianjin 300457, China,Tianjin State Key Laboratory of Modern Chinese Medicine, Tianjin University of Traditional Chinese Medicine, Tianjin 300193, China;Research and Development Center of Traditional Chinese Medicine, Tianjin International Joint Academy of Biotechnology and Medicine, Tianjin 300457, China,Tianjin State Key Laboratory of Modern Chinese Medicine, Tianjin University of Traditional Chinese Medicine, Tianjin 300193, China;Research and Development Center of Traditional Chinese Medicine, Tianjin International Joint Academy of Biotechnology and Medicine, Tianjin 300457, China and Tianjin State Key Laboratory of Modern Chinese Medicine, Tianjin University of Traditional Chinese Medicine, Tianjin 300193, China;Research and Development Center of Traditional Chinese Medicine, Tianjin International Joint Academy of Biotechnology and Medicine, Tianjin 300457, China |
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| Abstract: | |
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| Keywords: | Wenxin Keli HPLC Notoginsenoside R1 Ginsenoside Rg1 Lobetyolin Ginseno-side Rb1 Ginsenoside Rd |
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