| 赤芍挥发油成分的GC-MS分析 |
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| 引用本文： | 刘玉峰,刘洋,潘明辉,段洪云,陈立江. 赤芍挥发油成分的GC-MS分析[J]. 中国药房, 2011, 0(27): 2543-2545 |
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| 作者姓名： | 刘玉峰 刘洋 潘明辉 段洪云 陈立江 |
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| 作者单位： | 辽宁大学药学院; |
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| 基金项目： | 辽宁省自然科学基金项目(20092015); 辽宁大学青年科研基金入选项目(2009LDQN31);辽宁大学“211工程”三期学校重点学科建设项目 |
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| 摘 要： | 目的:分析赤芍中挥发油的化学成分,为其质量评价提供科学依据。方法:采用水蒸气蒸馏法提取赤芍挥发油,用气相色谱毛细管柱进行分析,归一化法测定其相对含量,并用气相色谱-质谱联用法鉴定化学成分。结果:检出134个色谱峰,鉴定出35个化合物,占挥发油总量的74.90%。其中n-十六烷酸、(Z,Z)-9,12-十八碳烯酸、油酸、十五烷酸、[1S-(1α,2α,5α)]-6,6-二甲基-二环[3.1.1]庚烷-2-甲醇、十六烷酸乙酯、9,12-十八碳烯酸乙酯、Z-β-松油基苯甲酸脂、1(-2-羟基-4-甲氧基苯基)-乙酮、(R)-1-甲烯基-3(-1-甲基-乙烯基)环己烷是主要成分,占挥发油总量的64.54%。结论:本试验为赤芍挥发油的进一步研究奠定了基础。
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| 关 键 词： | 赤芍 挥发油 气相色谱-质谱联用法 成分分析 |
GC-MS Analysis of Volatile Oil from Paeoniae Radix Rubra |
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| LIU Yu-feng,LIU Yang,PAN Ming-hui,DUAN Hong-yun,CHEN Li-jiang. GC-MS Analysis of Volatile Oil from Paeoniae Radix Rubra[J]. China Pharmacy, 2011, 0(27): 2543-2545 |
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| Authors: | LIU Yu-feng LIU Yang PAN Ming-hui DUAN Hong-yun CHEN Li-jiang |
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| Affiliation: | LIU Yu-feng,LIU Yang,PAN Ming-hui,DUAN Hong-yun,CHEN Li-jiang(College of Pharmacy,Liaoning University,Shenyang 110036,China) |
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| Abstract: | OBJECTIVE:To analyze the chemical constituents of volatile oils extracted from Paeoniae Radix Rubra,to provide scientific basis for quality evaluation of it.METHODS:Volatile oils were extracted from Paeoniae Radix Rubra by water-steam distillation and separated by GC capillary column chromatography.The components were quantitatively determined with normalization method,and were identified by GC-MS.RESULTS:134 peaks and 35 compounds were identified,accounting for 74.90% of the total volatile oils.n-hexadecan... |
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| Keywords: | Paeoniae Radix Rubra Volatile oil GC-MS Analysis of components |
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