| 香桂化浊胶囊的质量标准研究 |
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| 引用本文： | 刘红淼,杨继章,王云志,李艳玲,康丽娟.香桂化浊胶囊的质量标准研究[J].中国药房,2011(27):2553-2554. |
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| 作者姓名： | 刘红淼 杨继章 王云志 李艳玲 康丽娟 |
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| 作者单位： | 河北医科大学第一医院;河北医科大学;河北医科大学制药厂; |
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| 基金项目： | 河北省中医药管理局中医药类科研计划课题(2010009) |
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| 摘 要： | 目的:建立香桂化浊胶囊的质量标准。方法:采用薄层色谱(TLC)法鉴别香桂化浊胶囊中的土大黄和肉桂;用气相色谱法对君药广藿香中百秋李醇进行定量分析。结果:定性鉴别分离较好,专属性强;百秋李醇进样量在0.7656～3.8280μg范围内与峰面积积分值呈良好的线性关系(r=0.9999),平均回收率为99.17%,RSD=1.65%(n=6)。结论:所建标准可用于香桂化浊胶囊的质量控制。
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| 关 键 词： | 香桂化浊胶囊 质量标准 薄层色谱法 百秋李醇 气相色谱法 |
Quality Standard of Xianggui Huazhuo Capsule |
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| LIU Hong-miao,YANG Ji-zhang WANG Yun-zhi,LI Yan-ling KANG Li-juan.Quality Standard of Xianggui Huazhuo Capsule[J].China Pharmacy,2011(27):2553-2554. |
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| Authors: | LIU Hong-miao YANG Ji-zhang WANG Yun-zhi LI Yan-ling KANG Li-juan |
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| Institution: | LIU Hong-miao,YANG Ji-zhang(The First Hospital of Hebei Medical University,Shijiazhuang 050031,China) WANG Yun-zhi,LI Yan-ling(Hebei Medical University,Shijiazhuang 050017,China) KANG Li-juan(Hebei Medical University Pharmaceutical Factory,China) |
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| Abstract: | OBJECTIVE：To establish the quality standard of Xianggui huazhuo capsules.METHODS：Nepal Dock Root and Cinnamomum cassia in Xianggui huazhuo capsule were identified by TLC;Patchouli alcohol in the principal drug Herba Pogostemonis was analyzed quantitatively by GC.RESULTS：The qualitative identification is well-separated and specific.The linear range of patchouli alcohol was 0.765 6～3.828 0 μg（r=0.999 9） with an average recovery of 99.17%（RSD=1.65%,n=6）.CONCLUSION：Established standard is suitable for the quality control of Xianggui huazhuo capsule. |
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| Keywords: | Xianggui huazhuo capsule Quality standard TLC Patchouli alcohol GC |
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