| 健脾润肺片的质量标准研究 |
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| 引用本文： | 张志亮,吕杨.健脾润肺片的质量标准研究[J].中国药房,2011(27):2567-2570. |
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| 作者姓名： | 张志亮 吕杨 |
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| 作者单位： | 新乡医学院第一附属医院;河南大学药学院; |
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| 摘 要： | 目的:建立健脾润肺片的质量标准。方法:采用薄层色谱(TLC)法对处方中的当归、五味子、麦冬、黄芪、制何首乌、黄芩、陈皮进行定性鉴别,采用高效液相色谱法对本品中五味子醇甲进行含量测定。结果:TLC分离效果好,专属性强。五味子醇甲进样量在5～25μg范围内与峰面积积分值呈良好的线性关系(r=0.9999);平均回收率为99.44%,RSD=2.81%(n=6)。结论:所建标准可用于健脾润肺片的质量控制。
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| 关 键 词： | 健脾润肺片 质量标准 薄层色谱法 高效液相色谱法 五味子醇甲 |
Quality Standard of Jianpi Runfei Tablets |
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| ZHANG Zhi-liang LV Yang.Quality Standard of Jianpi Runfei Tablets[J].China Pharmacy,2011(27):2567-2570. |
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| Authors: | ZHANG Zhi-liang LV Yang |
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| Institution: | ZHANG Zhi-liang(The First Affiliated Hospital of Xinxiang Medical College,Xinxiang 453003,China) LV Yang(College of Pharmacy,Henan University,Kaifeng 475001,China) |
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| Abstract: | OBJECTIVE：To establish the quality standard of Jianpi runfei tablets.METHODS：Angelica sinensis,Schisandrae chinensis,Ophiopogon japoncius,Astragalus membranaceus,processed Polygonum multiflorum,Scutellaria baicalensis,Citrus reticulatae were identified by TLC,and the content of schisadrol A in the tablets was determined by HPLC.RESULTS：TLC spots were well-separated and specific.The linear range of schisadrol A were 5～25 μg（r=0.999 9） with an average recovery of 99.44%（RSD=2.81%,n=6）.CONCLUSION：The standard was used for the quality control of Jianpi runfei tablets. |
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| Keywords: | Jianpi runfei tablets Quality standard TLC HPLC Schisadrol A |
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