| 小茴香及其盐制品定性定量研究 |
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| 引用本文： | 邢俊波,曹红,陈玉敏,水彩红. 小茴香及其盐制品定性定量研究[J]. 中国中医药信息杂志, 2010, 17(8): 47-48. DOI: 10.3969/j.issn.1005-5304.2010.08.022 |
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| 作者姓名： | 邢俊波 曹红 陈玉敏 水彩红 |
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| 作者单位： | 中国人民解放军总后勤部卫生部药品仪器检验所,北京,100071 |
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| 基金项目： | 《中华人民共和国药典》2010版（一部）标准研究（YD-169） |
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| 摘 要： | 目的建立小茴香及盐小茴香的定性定量分析方法。方法采用薄层色谱法对小茴香及盐小茴香中茴香醛进行定性鉴别;采用气相色谱法测定其中反式茴香脑的含量。结果应用所建立的方法对多批样品进行定性与定量分析,结果TLC图谱斑点清晰,小茴香与盐小茴香中反式茴香脑的含量无明显差异。反式茴香脑在0.15～1.53μg范围内呈良好线性关系,平均回收率为99.17%(n=6)。结论本方法重复性好、简便易行,结果准确、可靠,可用于小茴香及盐小茴香的质量控制。
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| 关 键 词： | 小茴香 盐小茴香 薄层色谱法 气相色谱法 反式茴香脑 |
Study on Qualitative and Quantitative Analysis of Fennel and Prepared Fennel |
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| Affiliation: | XING Jun-bo,CAO Hong, CHEN Yu-min, et al (Institute for Drug and Instrument Control of Health Dept, GLD of PLA, Beijing 100071, China) |
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| Abstract: | Objective To establish a method for qualitative and quantitative analysis of Fennel andprepared Fennel. Method TLC was used for identification of anisealdehyde, and gas chromatographycarried out to determine the content of trans-anethole in Fennel and prepared Fennel. Results Thecalibration curve of trans-anethole was found to be linear in the range of 0.15～1.53 μg. The averagerecovery of trans- anethole was 99.17% （n =6）. Conclusion The method was simple, rapid and wellreproducible. It can be used as a reliable method for quality control of Fennel and prepared Fennel. |
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| Keywords: | Fennel prepared Fennel TLC GC trans-anethole |
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