| 蒙药旋覆花挥发油化学成分分析 |
| |
| 引用本文： | 李增春,杨利青,徐宁,张力,侯冬岩.蒙药旋覆花挥发油化学成分分析[J].药物分析杂志,2007,27(1):117-119. |
| |
| 作者姓名： | 李增春 杨利青 徐宁 张力 侯冬岩 |
| |
| 作者单位： | 内蒙古民族大学化学学院，鞍山师范学院 |
| |
| 基金项目： | 内蒙古教育厅高校科学基金资助项目,批准号ZD0016.致谢：本项研究工作得到鞍山师范学院回瑞华教授和李铁纯副教授的热诚帮助,特此致谢. |
| |
| 摘 要： | 目的:利用气相色谱-质谱联用技术对蒙药旋覆花挥发油化学成分进行全面分析。方法:使用乙醚萃取浓缩、水蒸气蒸馏的方法提取旋覆花挥发油,利用气相色谱-质谱联用技术分离鉴定,采用 GC 峰面积归一化法定量。结果:共鉴定出29个成分,占挥发油色谱总峰面积的90.35%,其中邻苯二甲酸二丁基酯16.30%,有6个化合物含量超过7%。结论:本方法快速方便,重现性好,适用于旋覆花挥发油化学成分分析。
|
| 关 键 词： | 旋覆花 挥发油 气相色谱-质谱 |
| 文章编号： | 0254-1793（2007）01-0117-03 |
| 修稿时间： | 2005-10-08 |
Study on chemical constituents of volatile oil from Inula japonica Thunb. from Nei Monggol |
| |
| LI Zeng - chun, YANG Li - qing, XU Ning, ZHANG Li, HOU Dong -yan.Study on chemical constituents of volatile oil from Inula japonica Thunb. from Nei Monggol[J].Chinese Journal of Pharmaceutical Analysis,2007,27(1):117-119. |
| |
| Authors: | LI Zeng - chun YANG Li - qing XU Ning ZHANG Li HOU Dong -yan |
| |
| Institution: | 1. College of Chemistry, Inner Mongolia University for the Nationalities ,Tongliao 028043, China; 2. Anshan Normal University, Anshan 114005, China |
| |
| Abstract: | Objective:To analyze the chemical components of volatile oil in Inula japonica Thunb.from Nei Monggol by GC-MS.Methods:The volatile oil from inula flower was extracted by ethyl ether,then isolated by steam distil- lation method.Their chemical constituents and relative contents was analyzed by GC-MS method.Results:Twenty nine volatile components of inula flower were separated and identified,which accounted for over 90.35% of total vola- tile oil fraction.In addition,dibutyl phthalate accounted for over 16.30% of total volatile oil fraction and six compounds' content overpassed 7%.Conclusion:The method is rapid,convenient and reproducible,therefore this method can be applied to the analysis of the volatile oil components,which was extracted from inula flower compo- nents. |
| |
| Keywords: | inula flower volatile oil GC-MS |
| 本文献已被 CNKI 维普 等数据库收录！ |
|
